1-苯基-1,4-戊二酮合成路线 (共 177 条)
反应条件
potassium cyanide in N,N-dimethyl-formamide 0.5 h; Ambient temperature;
参考文献
Miyashita; Suzuki; Okumura; Higashino
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 252 - 254
反应条件
in tetrahydrofuran T=-78°C; 0.416667 h;
参考文献
Kitahara, Haruo; Tozawa, Yasuyuki; Fujita, Seikou; Tajiri, Akio; Morita, Noboru; Asao, Toyonobu
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 9 p. 3362 - 3364
反应条件
Hg(OTf)2 in acetonitrile T=20°C; 0.25 h;
参考文献
Organic Letters, , vol. 6, # 21 p. 3679 - 3681
反应条件
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 40 min, 2.) THF, hexane, RT 2: Amberlyst-15, H2O / acetone 3: 50 percent / p-benzoquinone, PdCl2, H2O / dimethylformamide / 3 h / 70 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 115, # 3 p. 830 - 846
反应条件
1: Amberlyst-15, H2O / acetone 2: 50 percent / p-benzoquinone, PdCl2, H2O / dimethylformamide / 3 h / 70 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 115, # 3 p. 830 - 846
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; PtBu3*HBF4; N,N-dicyclohexylmethylamine in 1,4-dioxane T=85°C; Heck reaction; 16 h; Inert atmosphere;
参考文献
Proceedings of the National Academy of Sciences of the United States of America, , vol. 107, # 8 p. 3373 - 3376
反应条件
silver(l) oxide in dimethyl sulfoxide
参考文献
Journal of the American Chemical Society, , vol. 97, p. 649 - 651
反应条件
(acetylmethylene)triphenylphosphorane in dichloromethane T=20°C; Isomerization; 336000 h;
参考文献
Avery, Thomas D.; Taylor, Dennis K.; Tiekink, Edward R.T.
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5531 - 5546
反应条件
air; acetic acid T=23°C; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 6 p. 1800 - 1809
反应条件
potassium permanganate; silica gel in benzene Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2253 - 2258