双(三甲基硅基)过氧化物合成路线 （共 69 条）
反应条件
1,4-diaza-bicyclo[2.2.2]octane in dichloromethane T=0°C; 3 h;
参考文献
Taddei, Maurizio; Ricci, Alfredo
Synthesis, 1986 , # 8 p. 633 - 635
反应条件
oxygen in benzene T=80°C; 12 h;
参考文献
Journal of Organometallic Chemistry, , vol. 201, # 1 p. 197 - 211
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
in diethyl ether Ambient temperature-78 deg C to room temp.;
参考文献
Taddei, Maurizio; Ricci, Alfredo
Synthesis, 1986 , # 8 p. 633 - 635
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 30, # 28 p. 3721 - 3724
反应条件
sulfur trioxide in dichloromethane T=-30°C;
参考文献
Camporeale, Michele; Fiorani, Tiziana; Troisi, Luigino; Adam, Waldemar; Curci, Ruggero; Edwards, John O.
Journal of Organic Chemistry, 1990 , vol. 55, # 1 p. 93 - 98
反应条件
lithium bromide in diethyl ether T=0°C;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
参考文献
Taddei, Maurizio; Ricci, Alfredo
Synthesis, 1986 , # 8 p. 633 - 635
反应条件
in n-heptane T=-20°C; addition of lithium tert- butoxide or lithium trimethylsilanolate; KineticsMechanism;
参考文献
Baryshnikov, Yu. N.; Kurskii, Yu. A.; Kaloshina, N. N.; Vesnovskaya, G. I.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 10 p. 2288 - 2292,2037 - 2040
反应条件
hydrogen fluoride; SbF5 T=-70°C;
参考文献
Minkwitz, Rolf; Hirsch, Claudia; Hartl, Hans
Angewandte Chemie - International Edition, 1998 , vol. 37, # 12 p. 1681 - 1684
