1: 68 percent / BuLi / hexane; tetrahydrofuran / -100 °C
2: 57 percent / lithiumdiisopropylamide (LDA) / tetrahydrofuran / 2 h / -78 °C
3: 87 percent / LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature
View Scheme
参考文献
Shimizu, Nobujiro; Kinoshita, Chieko; Osajima, Erika; Hayakawa, Fumie; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 11 p. 3280 - 3288