环戊-1-烯-1-乙酸乙酯合成路线 （共 24 条）
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide
T=230°C; Wittig reaction; 0.333333 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Wu, Jinlong; Li, Dan; Wu, Huafeng; Sun, Lijie; Dai, Wei-Min
Tetrahedron, 2006 , vol. 62, # 19 p. 4643 - 4650
反应条件
pyridine; thionyl chloride
46 h; Title compound not separated from byproducts;
参考文献
Miyashi,T.; Nishizawa,Y.; Fujii,Y.
Journal of the American Chemical Society, 1986 , vol. 108, p. 1617
反应条件
1: naphthalenelithium / tetrahydrofuran / 0.08 h / -70 °C
2: dimethyl sulfate, sodium hydroxide; 20 percent sulfuric acid / H2O; toluene / 2 h / Ambient temperature
3: p-toluenesulfonic acid / benzene / 20 h / Heating
View Scheme
参考文献
Screttas, Constantinos G.; Smonou, Ioulia C.
Journal of Organometallic Chemistry, 1988 , vol. 342, p. 143 - 152
反应条件
1: 92 percent / potassium hydrogen sulfate / 120 °C
2: naphthalenelithium / tetrahydrofuran / 0.08 h / -70 °C
3: dimethyl sulfate, sodium hydroxide; 20 percent sulfuric acid / H2O; toluene / 2 h / Ambient temperature
4: p-toluenesulfonic acid / benzene / 20 h / Heating
View Scheme
参考文献
Screttas, Constantinos G.; Smonou, Ioulia C.
Journal of Organometallic Chemistry, 1988 , vol. 342, p. 143 - 152
反应条件
1: dimethyl sulfate, sodium hydroxide; 20 percent sulfuric acid / H2O; toluene / 2 h / Ambient temperature
2: p-toluenesulfonic acid / benzene / 20 h / Heating
View Scheme
参考文献
Screttas, Constantinos G.; Smonou, Ioulia C.
Journal of Organometallic Chemistry, 1988 , vol. 342, p. 143 - 152
反应条件
chloro-trimethyl-silane; lithium bromide in acetonitrile
Heating;
参考文献
Suri, Suresh C.; Marcischak, Jacob C.
Synthetic Communications, 2005 , vol. 35, # 3 p. 379 - 387
反应条件
(i) Zn-Hg, I2, benzene, toluene, (ii) P2O5; Multistep reaction;
参考文献
Hanack,M.; Schneider,H.-J.
Justus Liebigs Annalen der Chemie, 1965 , vol. 686, p. 8 - 18
参考文献
Kon; Linstead; Maclennan
Journal of the Chemical Society, 1932 , p. 2453
反应条件
T=100°C; Isomerisierung; Kinetics;
参考文献
Kon; Nargund
Journal of the Chemical Society, 1934 , p. 623,624, 625, 628
参考文献
Harding; Haworth
Journal of the Chemical Society, 1910 , vol. 97, p. 497
