N-(2-氨基乙基)环己胺合成路线 （共 8 条）
反应条件
sodium cyanoborohydride; acetic acid in methanol
Molecular sieve;
参考文献
Bersot, Ross; Humphries, Paul
Patent: US2013/303524 A1, 2013 ;
Location in patent: Paragraph 0484-0485 ;
反应条件
hydrogen
T=160°C; P=8250.83 Torr;
参考文献
Huang, Jia-Min; Xu, Lu-Feng; Qian, Chao; Chen, Xin-Zhi
Chemical Papers, 2012 , vol. 66, # 4 p. 304 - 307
反应条件
1: 1 h / 20 °C
2: NaB(OAc)3H / 24 h / 20 °C
View Scheme
参考文献
Rehse, Klaus; Steege, Jens
Archiv der Pharmazie, 2005 , vol. 338, # 11 p. 539 - 547
反应条件
hydrogen
T=200°C; P=7500.75 Torr; 8 h; Product distribution / selectivity;
参考文献
Tosoh Corporation
Patent: JP2005/41806 A, 2005 ;
Location in patent: Page/Page column 7; 8 ;
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Benko; Tisler
Croatica Chemica Acta, 1958 , vol. 30, p. 243
参考文献
Lehmann; Eckardt; Faust; Fiedler
Pharmazie, 1980 , vol. 35, # 5-6 p. 278 - 284
参考文献
Pearson; Jones; Cope
Journal of the American Chemical Society, 1946 , vol. 68, p. 1227
参考文献
Pearson; Jones; Cope
Journal of the American Chemical Society, 1946 , vol. 68, p. 1227
