1: With benzotriazol-1-ol; N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide 15 h; 2: With hydrogen; 5-palladium/activated carbon in ethanol T=200°C; 5.08333 h;
triethylamine in chloroform T=20°C; Substitution; 6 h;
参考文献
Canle, Moises L.; Clegg, William; Demirtas, Ibrahim; Elsegood, Mark R.J.; Maskill, Howard
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 1 p. 85 - 92
magnesium sulfate; triethylamine in dichloromethane 1 h; Heating;
参考文献
Mashchenko, N. V.; Matveeva, A. G.; Odinets, I. L.; Matrosov, E. I.; Petrov, E. S.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 9 p. 1973 - 1989,1762 - 1767
magnesium sulfate; triethylamine in dichloromethane 1 h; Heating;
参考文献
Mashchenko, N. V.; Matveeva, A. G.; Odinets, I. L.; Matrosov, E. I.; Petrov, E. S.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 9 p. 1973 - 1989,1762 - 1767