2-氧代-3-苯基-丙醛合成路线 （共 20 条）
反应条件
hydrogenchloride in ethanol T=80°C; 4 h;
参考文献
Qi, Chen Feng; Gomi, Yasushiro; Hirano, Takashi; Ohashi, Mamoru; Ohmiya, Yoshihiro; Tsuji, Frederick I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 13 p. 1607 - 1612
反应条件
toluene-4-sulfonic acid
参考文献
Dahn,H. et al.
Helvetica Chimica Acta, 1963 , vol. 46, p. 1000 - 1006
反应条件
pyridine; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol T=25°C; P=1748 Torr; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3011 - 3018
反应条件
pyridine; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol T=25°C; P=1748 Torr; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3011 - 3018
反应条件
pyridine; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol T=25°C; P=1748 Torr; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3011 - 3018
反应条件
pyridine; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol T=25°C; P=1748 Torr; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Jin, Shiow-Jen; Arora, Pramod K.; Sayre, Lawrence M.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3011 - 3018
反应条件
pyridine; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol T=25°C; P=1748 Torr; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3011 - 3018
反应条件
1: With pyridine; acetic anhydride
T=20°C; 15 h;
2: With hydrogenchloride in dichloromethane; water
参考文献
Promega Corporation
Patent: US7692022 B2, 2010 ;
Location in patent: Page/Page column 45-46 ;
US 7692022 B2
反应条件
water; toluene-4-sulfonic acid in tetrahydrofuran
20 h; Heating;
参考文献
Tiecco, Marcello; Testaferri, Lorenzo; Tingoli, Marco; Chianelli, Donatella; Bartoli, Donatella
Journal of Organic Chemistry, 1991 , vol. 56, # 14 p. 4529 - 4534
反应条件
perchloric acid in 1,4-dioxane
T=25°C;
参考文献
Dahn,H. et al.
Helvetica Chimica Acta, 1963 , vol. 46, p. 1000 - 1006
