3-(1,3-二噻烷-2-亚基)-2,4-戊二酮合成路线 （共 30 条）
参考文献
Yu, Haifeng; Liu, Qun; Yin, Yanbing; Fang, Qunxin; Zhang, Jingping; Dong, Dewen
Synlett, 2004 , # 6 p. 999 - 1002
反应条件
sulfuric acid in ethanol T=20°C;
参考文献
Dong, Dewen; Liu, Yingchun; Zhao, Yulong; Qi, Yimei; Wang, Zhuo; Liu, Qun
Synthesis, 2005 , # 1 art. no. F09904SS, p. 85 - 91
反应条件
water in ethanol Heating;
参考文献
Dong, Dewen; Liu, Yingchun; Zhao, Yulong; Qi, Yimei; Wang, Zhuo; Liu, Qun
Synthesis, 2005 , # 1 art. no. F09904SS, p. 85 - 91
反应条件
1: carbon disulfide; acetylacetone With tetrabutylammomium bromide; potassium carbonate in water T=20°C; 1 h; 2: X-(CH2)3-X, X = Hal in water T=20°C; 8.25 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 73, # 19 p. 7625 - 7630
参考文献
Liu, Qun; Che, Guangbo; Yu, Haifeng; Liu, Yingchun; Zhang, Jingping; Zhang, Qian; Dong, Dewen
Journal of Organic Chemistry, 2003 , vol. 68, # 23 p. 9148 - 9150
反应条件
acetyl chloride in methanol 6 h; Heating;
参考文献
Yu, Haifeng; Liu, Qun; Yin, Yanbing; Fang, Qunxin; Zhang, Jingping; Dong, Dewen
Synlett, 2004 , # 6 p. 999 - 1002
反应条件
hydrogenchloride T=60°C; 0.416667 h;
参考文献
Synthesis, , # 22 p. 3801 - 3804
反应条件
hydrogenchloride T=60°C; 1 h;
参考文献
Ouyang, Yan; Dong, Dewen; Zheng, Chunbai; Yu, Haifeng; Liu, Qun; Fu, Zhenqian
Synthesis, 2006 , # 22 p. 3801 - 3804
反应条件
1: 92 percent / Mg / methanol / 24 h / 5 °C 2: 45 percent / ethanol / 3 h / Heating View Scheme
参考文献
Mellor, John M.; Schofield, Stephen R.; Korn, Stewart R.
Tetrahedron, 1997 , vol. 53, # 50 p. 17151 - 17162
反应条件
1: 92 percent / Mg / methanol / 24 h / 5 °C 2: 99 percent / NH2OH*HCl / ethanol / 2 h / Heating View Scheme
参考文献
Mellor, John M.; Schofield, Stephen R.; Korn, Stewart R.
Tetrahedron, 1997 , vol. 53, # 50 p. 17151 - 17162
