2,2,6-三甲基-4H-1,3-二英-4-酮合成路线 （共 203 条）
参考文献
Sato, Masayuki; Ogasawara, Hiromischi; Kato, Keiko; Sakai, Masako; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4300 - 4305
反应条件
in toluene
0.5 h; Heating;
参考文献
Sato, Masayuki; Ogasawara, Hiromischi; Kato, Keiko; Sakai, Masako; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4300 - 4305
反应条件
in xylene
1 h; Heating;
参考文献
Sunkel, Carlos E.; Casa-Juana, Miguel Fau de; Santos, Luis; Gomez, M. Mar; Villarroya, Mercedes; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 12 p. 3205 - 3210
反应条件
in xylene
T=150°C; 0.5 h;
参考文献
Clemens, Robert J.; Hyatt, John A.
Journal of Organic Chemistry, 1985 , vol. 50, # 14 p. 2431 - 2435
反应条件
in xylene
0.666667 h; Heating;
参考文献
Hyatt, John A.; Feldman, Paul L.; Clemens, Robert J.
Journal of Organic Chemistry, 1984 , vol. 49, # 26 p. 5105 - 5108
反应条件
in xylene
T=130°C; 1 h;
参考文献
Sato, Masayuki; Ogasawara, Hiromichi; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 7 p. 2602 - 2608
反应条件
in toluene
3 h; Inert atmosphereHeating;
参考文献
Rossbach, Jan; Baumeister, Julia; Harms, Klaus; Koert, Ulrich
European Journal of Organic Chemistry, 2013 , # 4 p. 662 - 665
参考文献
Bayer HealthCare AG
Patent: US2009/214675 A1, 2009 ;
反应条件
in anhydrous xylene
Reflux;
参考文献
Razzaghi-Asl, Nima; Firuzi, Omidreza; Hemmateenejad, Bahram; Javidnia, Katayoun; Edraki, Najmeh; Miri, Ramin
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 22 p. 6893 - 6909
反应条件
1: 2,2,6-trimethyl-4H-1,3-dioxin-4-one; allyl alcohol in tetrahydrofuran
Heating;
2: 4-Acetylaminobenzenesulfonyl Azide in acetonitrile
T=20°C;
3: With lithium hydroxide
参考文献
Brana, Miguel F; Guisado, Cristina; Fernando Alguacil, Luis; Garrido, Elisa; Perez-Garcia, Carmen; Ruiz-Gayo, Mariano
Bioorganic and medicinal chemistry letters, 2002 , vol. 12, # 24 p. 3561 - 3563
