in methanol byproducts: LiCl; under N2, to methanol soln. of LiOMe added (CH3)3CSH and filtered soln.of FeCl3 in CH3OH, anhyd. Li2S added to this mixt., heated at 55°C for 1-2 h, stirred overnight at ambient temp., filtered into methanolsoln. of (Me3NCH2Ph)Br; filtered, recrystd. from Me2SO/MeOH (1:1), elem. anal.;
参考文献
Christou, G.; Sabat, M.; Ibers, James A.; Holm, R.H.
Inorganic Chemistry, 1982 , vol. 21, p. 3518 - 3526
