1-苯基戊烷-1,3-二酮合成路线 （共 36 条）
反应条件
anhydrous iron chloride; tert.-butylnitrite T=30°C; 12 h; Under airNeat (no solvent);
参考文献
Journal of Organic Chemistry, , vol. 76, # 14 p. 5732 - 5737
反应条件
sodium hydride 1.) THF, reflux, 30 min, 2.) THF, reflux 2 h; Yield given. Multistep reaction;
参考文献
Davis, Brian R.; Hinds, Mark G.; Ting, Philip P. C.
Australian Journal of Chemistry, 1992 , vol. 45, # 5 p. 865 - 875
参考文献
Leser
Bulletin de la Societe Chimique de France, 1902 , vol. <3> 27, p. 68
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1909 , vol. 149, p. 1080
反应条件
water; Aliquatreg; 336; PtCl4-CO in various solvent(s)
T=110°C; P=1034.3 Torr; 9 h;
参考文献
Baidossi, Wael; Lahav, Michal; Blum, Jochanan
Journal of Organic Chemistry, 1997 , vol. 62, # 3 p. 669 - 672
反应条件
sodium hydride
3.5 h; Ambient temperature;
参考文献
Davis, Brian R.; Hinds, Mark G.; Ting, Philip P. C.
Australian Journal of Chemistry, 1992 , vol. 45, # 5 p. 865 - 875
反应条件
samarium (III) iodide in acetonitrile
0.5 h; Ambient temperature;
参考文献
Chen, Rener; Wu, Huayue; Zhang, Yongmin
Journal of Chemical Research - Part S, 1999 , # 11 p. 666 - 667
反应条件
samarium (III) iodide in acetonitrile
1 h; Ambient temperature;
参考文献
Ying, TaoKai; Bao, Weiliang; Zhang, Yongmin
Synthetic Communications, 1996 , vol. 26, # 15 p. 2905 - 2909
反应条件
carbon monoxide; water; platinum (IV)-chloride in tetrahydrofuran
T=80°C; P=1034.3 Torr; 5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Baidossi, Wael; Lahav, Michal; Blum, Jochanan
Journal of Organic Chemistry, 1997 , vol. 62, # 3 p. 669 - 672
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; cataCXium®A; caesium carbonate
T=60°C; P=2250.23 Torr; 36 h; GloveboxInert atmosphereAutoclave;
参考文献
Schranck, Johannes; Tlili, Anis; Alsabeh, Pamela G.; Neumann, Helfried; Stradiotto, Mark; Beller, Matthias
Chemistry - A European Journal, 2013 , vol. 19, # 38 p. 12624 - 12628
反应条件
potassium 2-methyl-2-butoxide in tetrahydrofuran; toluene
参考文献
Simunek, Petr; Svobodova, Marketa; Bertolasi, Valerio; Machacek, Vladimir
Synthesis, 2008 , # 11 p. 1761 - 1766
