吡啶-2-基氨基甲酸乙酯合成路线 (共 20 条)
反应条件
1: acetic acid; aqueous H2O2 / Erhitzen mit konz. wss. HCl und Behandeln mit aethanol. Natriumaethylat 2: acetonitrile 3: ethanol View Scheme
参考文献
Katritzky
Journal of the Chemical Society, 1957 , p. 191,197
参考文献
Meyer,H.; Mally
Monatshefte fuer Chemie, 1912 , vol. 33, p. 395
反应条件
aluminum oxide; tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in neat (no solvent) T=140°C; 0.333333 h; Microwave irradiationGreen chemistry;
参考文献
Basolo, Luca; Bernasconi, Alice; Broggini, Gianluigi; Gazzola, Silvia; Beccalli, Egle M.
Synthesis (Germany), 2013 , vol. 45, # 22 art. no. SS-2013-Z0383-OP, p. 3151 - 3156
反应条件
pyridine 144 h; Heating;
参考文献
Luening, Ulrich; Kuehl, Christine; Uphoff, Andreas
European Journal of Organic Chemistry, 2002 , # 23 p. 4063 - 4070
反应条件
dihydrogen peroxide; acetic acid Erhitzen mit konz. wss. HCl und Behandeln mit aethanol. Natriumaethylat;
参考文献
Katritzky
Journal of the Chemical Society, 1957 , p. 191,197
反应条件
1: acetic acid; aqueous H2O2 / Erhitzen mit konz. wss. HCl und Behandeln mit aethanol. Natriumaethylat
2: acetonitrile
View Scheme
参考文献
Katritzky
Journal of the Chemical Society, 1957 , p. 191,197
反应条件
dihydrogen peroxide; acetic acid
参考文献
Katritzky
Journal of the Chemical Society, 1957 , p. 191,197
反应条件
yttria-zirconia based Lewis acid catalyst in acetonitrile
T=20°C; 0.25 h;
参考文献
Pandey, Rajesh K.; Dagade, Sharda P.; Dongare, Mohan K.; Kumar, Pradeep
Synthetic Communications, 2003 , vol. 33, # 23 p. 4019 - 4027
反应条件
T=0 - 20°C; 4 h; Inert atmosphere;
参考文献
Shewalkar, Mukesh P.; Rao, Ramakrishna R.; Reddy, Veerbhadra; Darandale, Sunil N.; Shinde, Devanand B.
Letters in Organic Chemistry, 2013 , vol. 10, # 1 p. 60 - 64
反应条件
iodine; oxygen; palladium diacetate; potassium carbonate
T=100°C; P=2585.7 Torr; 0.5 h;
参考文献
Pri-Bar, Ilan; Schwartz, Jeffrey
Journal of Organic Chemistry, 1995 , vol. 60, # 25 p. 8124 - 8125