2-氰基-3,3-二苯基丙烯酸乙酯合成路线 （共 10 条）
反应条件
acetic acid; 3-aminopropionic acid in benzene Knoevenagel condensation; 90 h; Heating;
参考文献
Gholap, Atul R.; Paul, Vincent; Srinivasan, Kumar V.
Synthetic Communications, 2008 , vol. 38, # 17 p. 2967 - 2982
参考文献
Charles
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1956 , vol. 242, p. 2468
参考文献
Karlsson, Isabella; Persson, Elin; Martensson, Jerker; Boerje, Anna
Photochemistry and Photobiology, 2012 , vol. 88, # 4 p. 904 - 912
参考文献
Cope et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 3455
反应条件
water; sodium chloride in dimethyl sulfoxide T=160 - 170°C; Krapcho decarboxylation; 4 h;
参考文献
Gholap, Atul R.; Paul, Vincent; Srinivasan, Kumar V.
Synthetic Communications, 2008 , vol. 38, # 17 p. 2967 - 2982
反应条件
in toluene T=100°C; 72 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 39, # 4 p. 559 - 573
反应条件
in diethyl ether T=23°C; 2.5 h; various solvents, time, temperature; Product distribution;
参考文献
Feit, Ben-Ami; Shapira, Sarit; Herbst, Amatzya
Tetrahedron, 1995 , vol. 51, # 1 p. 317 - 328
反应条件
1: With water; sodium hydroxide in methanol T=20°C; 2: With hydrogenchloride in methanol; water
参考文献
BASF SE
Patent: US2011/237665 A1, 2011 ;
Location in patent: Page/Page column 8 ;
反应条件
1: sodium hydroxide; water / methanol / 20 °C 2: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 25 h / 20 °C / Reflux View Scheme
参考文献
BASF SE
Patent: US2011/237665 A1, 2011 ;
