1,2-二(4-氯苯基)乙烷合成路线 (共 79 条)
反应条件
potassium permanganate in water; ethyl acetate 6 h; Reflux;
参考文献
WO2012/128965 A2, ;
Page/Page column 16 ;
反应条件
[C12mim][CuCl2]; copper; zinc
T=70°C; 2 h;
参考文献
Hu, Yu-Lin; Li, Fu; Gu, Guo-Liang; Lu, Ming
Catalysis Letters, 2011 , vol. 141, # 3 p. 467 - 473
反应条件
copper(I) bromide in water
T=20°C; 0.416667 h; under air;
参考文献
Shekarriz, Marzieh; Adib, Mehdi; Biabani, Tayebe; Taghipoor, Sohrab
Journal of Chemical Research, 2012 , vol. 36, # 1 p. 29 - 30
反应条件
bromine in ethyl acetate
1.5 h;
参考文献
Ding, Qingjie; Graves, Bradford James; Kong, Norman; Liu, Jin-Jun; Lovey, Allen John; Pizzolato, Giacomo; Roberts, John Lawson; So, Sung-Sau; Vu, Binh Thanh; Wovkulich, Peter Michael
Patent: US2007/129416 A1, 2007 ;
Location in patent: Page/Page column 65/1 ;
反应条件
di-tert-butyl peroxide
unter Stickstoff;
参考文献
Beckwith; Waters
Journal of the Chemical Society, 1957 , p. 1665,1667
反应条件
nickel in ethylene glycol dimethyl ether
T=70°C; 0.5 h;
参考文献
Inaba, Shin-ichi; Matsumoto, Hideyuki; Rieke, Reuben D.
Journal of Organic Chemistry, 1984 , vol. 49, # 12 p. 2093 - 2098
反应条件
sodium tetrahydroborate; nickel dichloride in methanol
T=20°C; 0.666667 h;
参考文献
Khurana, Jitender M.; Kandpal, Bhaskar M.; Kukreja, Gagan; Sharma, Purnima
Canadian Journal of Chemistry, 2006 , vol. 84, # 8 p. 1019 - 1023
反应条件
carbon monoxide; copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
-78 deg C, 2 h; room temp., 1 h; 60 deg C, 19 h;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
反应条件
carbon monoxide; methyl 2-iodobenzoate; copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
P=760 Torr; -78 deg C, 2h; room temp., 1 h; 60 deg C, 6 h; Further byproducts given;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
反应条件
zeolite Ca Y in hexane
T=22°C; 1 h; Yield given;
参考文献
Pitchumani; Joy, Abraham; Prevost, Nicolette; Ramamurthy
Chemical Communications, 1997 , # 1 p. 127 - 128