(乙氧基羰基甲基)二甲基溴化硫鎓合成路线 （共 32 条）
反应条件
in acetone T=15 - 22°C; 18 h;
参考文献
SLIL Biomedical Corporation
Patent: US2003/195377 A1, 2003 ;
Location in patent: Page/Page column 9-10 ;
反应条件
dimethylsulfide in acetone
参考文献
Eli Lilly and Company
Patent: US5661184 A1, 1997 ;
US 5661184 A
反应条件
1: (Ethoxycarbonylmethyl)dimethyl-sulfonium bromide With caesium carbonate in anhydrous xylene T=20°C; 2: N-(2-(chloromethyl)phenyl)-4-methylbenzenesulfonamide in anhydrous xylene T=20°C; 96 h;
参考文献
Yang, Qing-Qing; Xiao, Cong; Lu, Liang-Qiu; An, Jing; Tan, Fen; Li, Bin-Jie; Xiao, Wen-Jing
Angewandte Chemie - International Edition, 2012 , vol. 51, # 36 p. 9137 - 9140
反应条件
sodium hydride 1.) DMSO, rt., both educts were treated separately with reagent; 2.) DMSO, 80 deg C, 6 h; Yield given. Multistep reaction;
参考文献
Croce, Piero Dalla; Ferraccioli, Raffaella; La Rosa, Concetta
Heterocycles, 1996 , vol. 43, # 11 p. 2397 - 2407
反应条件
1: Me2S / dimethylsulfoxide View Scheme
参考文献
Labuschagne,A.J.H. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1978 , p. 955 - 961
反应条件
Yield given. Multistep reaction;
参考文献
Deng, Min-Zhi; Li, Nan-Sheng; Huang, Yao-Zeng
Journal of Organic Chemistry, 1992 , vol. 57, # 14 p. 4017 - 4019
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in tetrahydrofuran T=20°C; 4 h;
参考文献
Galin, F. Z.; Iskandarova, V. N.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 708 - 712
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 4 p. 828 - 833
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in tetrahydrofuran T=20°C; 4 h;
参考文献
Galin, F. Z.; Iskandarova, V. N.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 708 - 712
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 4 p. 828 - 833
反应条件
(i) BH3, (ii) /BRN= 4161472/, NaH, (iii) aq. H2O2, NaOH; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 89, # 25 p. 6804 - 6805
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in tetrahydrofuran T=20°C; 4 h;
参考文献
Galin, F. Z.; Iskandarova, V. N.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 708 - 712
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 4 p. 828 - 833
