1-氯-4-(苯基乙炔基)苯合成路线 （共 58 条）
反应条件
[Fe(II)(C5H5)(C5H4PPh2)]; gold monoiodide; potassium carbonate in toluene
T=130°C; Sonogashira reaction; 24 h;
参考文献
Li, Pinhua; Wang, Lei; Wang, Min; You, Feng
European Journal of Organic Chemistry, 2008 , # 35 p. 5946 - 5951
反应条件
copper(l) iodide; 8-hydroxy-quinoline; sodium salt of phosphorous acid in ethanol
T=80°C; Suzuki coupling; 24 h;
参考文献
Wang, Shihua; Wang, Min; Wang, Lei; Wang, Bo; Li, Pinhua; Yang, Jin
Tetrahedron, 2011 , vol. 67, # 26 p. 4800 - 4806
反应条件
potassium acetate; palladium diacetate; silver(l) oxide in dichloromethane
T=20°C; 12 h; Molecular sieve;
参考文献
Feng, Chao; Loh, Teck-Peng
Chemical Communications, 2010 , vol. 46, # 26 p. 4779 - 4781
反应条件
potassium phosphate; copper(l) iodide; 8-hydroxy-quinoline in ethanol
T=100°C; Suzuki Coupling; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Liu, Jidan; Dai, Fenglin; Yang, Zhiyong; Wang, Sizhuo; Xie, Kai; Wang, Anwei; Chen, Xiang; Tan, Ze
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5678 - 5683
反应条件
caesium carbonate; PdCl(C6H3-2,6-(OPiPr2)); zinc(II) chloride in 1,4-dioxane
T=160°C; 24 h;
参考文献
Eberhard, Michael R.; Wang, Zhaohui; Jensen, Craig M.
Chemical Communications, 2002 , # 8 p. 818 - 819
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in water
T=25°C; Sonogashira Cross-Coupling; P=760.051 Torr; 24 h; Green chemistry;
参考文献
Zhao, Hong; Cheng, Mingzhu; Zhang, Jiatao; Cai, Mingzhong
Green Chemistry, 2014 , vol. 16, # 5 p. 2515 - 2522
反应条件
sodium perchlorate; palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 4-BzO-TEMPO in water; acetonitrile
T=20°C; Inert atmosphereElectrochemical reaction;
参考文献
Mitsudo, Koichi; Shiraga, Takuya; Mizukawa, Jun-Ichi; Suga, Seiji; Tanaka, Hideo
Chemical Communications, 2010 , vol. 46, # 48 p. 9256 - 9258
反应条件
copper(l) iodide; tetrabutylammomium bromide; potassium carbonate; triphenylphosphine; sodium iodide in water
T=120°C; 48 h; Inert atmosphere;
参考文献
Li, Tingyi; Sun, Peng; Yang, Hailong; Zhu, Yan; Yan, Hong; Lu, Linhua; Mao, Jincheng
Tetrahedron, 2012 , vol. 68, # 32 p. 6413 - 6419
反应条件
copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; (benzyl)-tri-(butyl)-ammonium chloride; sodium hydroxide; [(t-Bu)3PH]BF4 in water; toluene
T=40°C; Sonogashira coupling; 22 h; Inert atmosphere;
参考文献
Bellina, Fabio; Lessi, Marco
Synlett, 2012 , vol. 23, # 5 p. 773 - 777
反应条件
4-(MeOPEG2000OCH2)C6H4CH2P(1-Ad)2*HBr; diisopropylamine; sodium tetrachloropalladium (II); copper(l) iodide in n-heptane; dimethyl sulfoxide
T=60°C; Sonogashira coupling; 1 h;
参考文献
Koellhofer, Axel; Plenio, Herbert
Chemistry - A European Journal, 2003 , vol. 9, # 6 p. 1416 - 1425
