N-亚苄基-4-甲基苯磺酰胺合成路线 （共 129 条）
反应条件
sodium hydride in tetrahydrofuran T=-40°C; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Dokli, Irena; Matanovic, Ivana; Hamersak, Zdenko
Chemistry - A European Journal, 2010 , vol. 16, # 38 p. 11744 - 11752
反应条件
dirhodium tetraacetate; dimethylsulfide Yield given. Yields of byproduct given;
参考文献
Aggarwal, Varinder K.; Thompson, Alison; Jones, Ray V. H.; Standen, Mike C. H.
Journal of Organic Chemistry, 1996 , vol. 61, # 24 p. 8368 - 8369
反应条件
[bis(acetoxy)iodo]benzene; potassium tert-butylate; tetrabutylammomium bromide in acetonitrile T=0 - 30°C;
参考文献
Fan, Renhua; Ye, Yang
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 10 p. 1526 - 1530
反应条件
dimethyl sulfoxide T=20°C; Knoevenagel condensation; 2.5 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Chiba, Ryoichi; Oriyama, Takeshi
Chemistry Letters, 2008 , vol. 37, # 12 p. 1218 - 1219
反应条件
air; boron trifluoride diethyl etherate; dimethyl zinc; copper(II) bis(trifluoromethanesulfonate) in hexane; dichloromethane T=0°C; 0.75 h;
参考文献
Yamada, Ken-Ichi; Yamamoto, Yasutomo; Maekawa, Masaru; Akindele, Tito; Umeki, Hiroyuki; Tomioka, Kiyoshi
Organic Letters, 2006 , vol. 8, # 1 p. 87 - 89
反应条件
1: hex-1-yne With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N-benzylidene-4-methylbenzenesulfonamide in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Ma, Shengming; Wu, Bin; Jiang, Xuefeng
Journal of Organic Chemistry, 2005 , vol. 70, # 7 p. 2588 - 2593
反应条件
1: triphenylbenzyl-phosphonium bromide in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: N-benzylidene-4-methylbenzenesulfonamide in tetrahydrofuran; hexane T=-78 - 20°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Dong, De-Jun; Li, Hai-Hua; Tian, Shi-Kai
Journal of the American Chemical Society, 2010 , vol. 132, # 14 p. 5018 - 5020
反应条件
1: With 1,2-di-iodoethane; zinc in tetrahydrofuran
T=43°C; Reformatsky Reaction; 2 h; Sonication;
2: With hydrogenchloride in water
Reformatsky Reaction;
参考文献
Lee, Adam Shih-Yuan; Chang, Yu-Ting; Su, Feng-Yi
Journal of the Chinese Chemical Society, 2014 , vol. 61, # 2 p. 290 - 294
反应条件
neodymium trifluoromethanesulfonate
T=20°C;
参考文献
Temelli, Baris; Unaleroglu, Canan
Tetrahedron, 2006 , vol. 62, # 43 p. 10130 - 10135
反应条件
in dimethyl sulfoxide
T=100°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
