2,3-二甲基-1,3-丁二烯合成路线 (共 777 条)
反应条件
hydrogen T=425°C; P=760.051 Torr; Gas phase;
参考文献
Sato, Satoshi; Sato, Natsumi; Yamada, Yasuhiro
Chemistry Letters, 2012 , vol. 41, # 8 p. 831 - 833
反应条件
tetrachloromethane; triphenylphosphine in acetonitrile 24 h; Heating; Title compound not separated from byproducts;
参考文献
Barry, Carey N.; Evans, Slayton A.
Tetrahedron Letters, 1983 , vol. 24, # 7 p. 661 - 664
参考文献
Richter, Frank U.
Chemistry - A European Journal, 2009 , vol. 15, # 21 p. 5200 - 5202
反应条件
pyridine; N,N'-dimethyl-N,N'-propyleneurea; 4,4'-dimethoxy-2,2'-bipyridine; NiI2*3.5H2O; sodium iodide; zinc T=20 - 60°C; 25 h; chemoselective reaction;
参考文献
Everson, Daniel A.; Jones, Brittany A.; Weix, Daniel J.
Journal of the American Chemical Society, 2012 , vol. 134, # 14 p. 6146 - 6159
反应条件
1: 2,3-dimethylbutane-2,3-diol With hydrogen bromide Reflux; 2: hydroquinone
参考文献
Mikhalitsyna, Elena A.; Tyurin, Vladimir S.; Nefedov, Sergey E.; Syrbu, Sergey A.; Semeikin, Aleksandr S.; Koifman, Oskar I.; Beletskaya, Irina P.
European Journal of Inorganic Chemistry, 2012 , # 36 p. 5979 - 5990
反应条件
in pentane T=23°C; Irradiation; Further byproducts given;
参考文献
Fahie, Brian J.; Leigh, William J.
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1859 - 1867
反应条件
T=400 - 1000°C; P=0.0001 - 1 Torr;
参考文献
Khabashesku, V. N.; Kerzina, Z. A.; Baskir, E. G.; Maltsev, A. K.; Nefedov, O. M.
Journal of Organometallic Chemistry, 1988 , vol. 347, p. 277 - 294
反应条件
aluminum oxide; Catalyst M-Chromium oxide; nitrogen T=590°C;
参考文献
Phillips Petr.Co.
Patent: US2438315 , 1944 ;
反应条件
phenylammonium bromide T=120°C;
参考文献
Addy; Baker
Journal of the Chemical Society, 1953 , p. 4111
反应条件
benzaldehyde T=600°C; Title compound not separated from byproducts;
参考文献
Marchand, Annette; Gerval, Pierre; Duboudin, Francoise; Gaufryau, M.-H.; Joanny, Marguerite; Mazerolles, Pierre
Journal of Organometallic Chemistry, 1984 , vol. 267, # 1 p. 93 - 106