反应条件
n-butyllithium in hexane
under Ar, BuLi in hexane added to PhC2H (slightly more than 1 equiv.) at 0°C, after 10 min Et2AlCl hexane soln. added, stirred for 15 min at 0°C; concd. in vac. below room temp.;
参考文献
Hiyama, Tamejiro; Morizawa, Yoshitomi; Yamamoto, Hajime; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 7 p. 2151 - 2160