1-氯-3-甲基-2-丁烯合成路线 （共 287 条）
参考文献
Huntsman et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 5455,5458
反应条件
1: dibenzoyl peroxide; SO2Cl2 2: quinoline / 170 °C View Scheme
参考文献
Ultee
Recueil des Travaux Chimiques des Pays-Bas, 1949 , vol. 68, p. 130
反应条件
toluene-4-sulfonic acid in toluene 3 h; Heating;
参考文献
Jetter; Heindel; Laskin
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 4 p. 995 - 997
反应条件
in N,N-dimethyl-formamide
参考文献
Lenevich, Stepan; Xu, Juhua; Hosokawa, Ayako; Cramer, Christopher J.; Distefano, Mark D.
Journal of the American Chemical Society, 2007 , vol. 129, # 18 p. 5796 - 5797
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
参考文献
Plemenkov, V. V.; Zverev, V. V.; Balakireva, E. G.; Appolonova, S. A.
Russian Journal of General Chemistry, 1994 , vol. 64, # 10.1 p. 1485 - 1488
Zhurnal Obshchei Khimii, 1984 , vol. 64, # 10 p. 1668 - 1671
反应条件
1: (i) NaOEt, EtOH, (ii) /BRN= 878156/ 2: (i) KOH, EtOH, H2O, (ii) Cu, quinoline, (heating) 3: (COCl)2 / petroleum ether 4: diethyl ether 5: Cu / cyclohexane / Heating View Scheme
参考文献
Julia,S.; Linstrumelle,G.
Bulletin de la Societe Chimique de France, 1966 , p. 3490 - 3498
反应条件
in N,N-dimethyl-formamide T=20°C;
参考文献
Journal of Fluorine Chemistry, , vol. 128, # 10 p. 1198 - 1215
反应条件
sodium hydroxide in water
参考文献
Kuraray Co., Ltd.
Patent: US4122119 A1, 1978 ;
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in benzene T=40°C; other reagent; MechanismProduct distribution;
参考文献
Yufit, S. S.; Esikova, I. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 9 p. 1637 - 1642
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , vol. 30, # 9 p. 1996 - 2001
反应条件
2-Chloro-2-methylpropane; lithium 1.) THF, 1h, reflux 2.) THF, 30 min; Yield given. Multistep reaction;
参考文献
Khachatryan, R. A.; Sayadyan, S. V.; Ovakimyan, M. Zh.; Indzhikyan, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 2.1 p. 313 - 315,267 - 269
