1,4-二氧六环-2,5-二酮合成路线 （共 26 条）
反应条件
1: in water T=110°C; 80 h; 2: With ethylene glycol; titanium tetraethoxide in 2-methoxy-ethanol; water T=185 - 215°C; P=2.25023 - 150.015 Torr; Product distribution / selectivity;
参考文献
SOLVAY SA; WAUTIER, Henri Georges Ghislain; MARCHAND, Dominique Francois Achille
Patent: WO2012/7379 A1, 2012 ;
Location in patent: Page/Page column 7-8 ;
反应条件
1: methanol; ethylene glycol With oxygen T=90°C; P=3750.38 Torr; 5 h; Autoclave; 2: glycolic acid ; magnesium glycolate in methanol T=80°C; 2 h; Autoclave;
参考文献
Hayashi, Toshio; Baba, Hideyuki
Patent: US2004/138409 A1, 2004 ;
Location in patent: Page 21-23 ;
反应条件
toluene-4-sulfonic acid in cyclohexane 5 h; Reflux;
参考文献
Jiang, Xiaoyan; Tang, Ying
Asian Journal of Chemistry, 2013 , vol. 25, # 15 p. 8447 - 8450
反应条件
toluene-4-sulfonic acid in cyclohexane 5 h; Reflux;
参考文献
Jiang, Xiaoyan; Tang, Ying
Asian Journal of Chemistry, 2013 , vol. 25, # 15 p. 8447 - 8450
反应条件
toluene-4-sulfonic acid in cyclohexane 5 h; Reflux;
参考文献
Jiang, Xiaoyan; Tang, Ying
Asian Journal of Chemistry, 2013 , vol. 25, # 15 p. 8447 - 8450
反应条件
toluene-4-sulfonic acid in cyclohexane 5 h; Reflux;
参考文献
Jiang, Xiaoyan; Tang, Ying
Asian Journal of Chemistry, 2013 , vol. 25, # 15 p. 8447 - 8450
反应条件
toluene-4-sulfonic acid in cyclohexane 5 h; Reflux;
参考文献
Jiang, Xiaoyan; Tang, Ying
Asian Journal of Chemistry, 2013 , vol. 25, # 15 p. 8447 - 8450
反应条件
toluene-4-sulfonic acid in cyclohexane 5 h; Reflux;
参考文献
Jiang, Xiaoyan; Tang, Ying
Asian Journal of Chemistry, 2013 , vol. 25, # 15 p. 8447 - 8450
反应条件
copper-turnings T=300°C; P=5 Torr;
参考文献
Sporzynski; Kocay; Briscoe
Recueil des Travaux Chimiques des Pays-Bas, 1949 , vol. 68, p. 614
反应条件
benzene nachfolgend Schuetteln der Loesung mit Wasser;
参考文献
Gold-; Silberscheideanst
Patent: DE379752 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 293
