1,6-脱水-β-D-葡萄糖合成路线 （共 127 条）
反应条件
water T=90°C; 3 h; Inert atmosphere;
参考文献
Hu, Xun; Li, Chun-Zhu
Green Chemistry, 2011 , vol. 13, # 7 p. 1676 - 1679
参考文献
Wolfrom; Montgomery
Journal of the American Chemical Society, 1950 , vol. 72, p. 2859
参考文献
Bulletin des Societes Chimiques Belges, , vol. 91, # 4 p. 297 - 300
反应条件
4 A molecular sieve; di(n-butyl)tin oxide; triethylamine 1.) benzene, reflux, 4h; 2.) 1,2-dimethoxyethane, 2 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Grindley, T. Bruce; Thangarasa, Rasiah
Carbohydrate Research, 1988 , vol. 172, p. 311 - 318
反应条件
H-MCM-36-P22-28 zeolite T=299.84°C; P=760.051 Torr; Gas phase;
参考文献
Kaeldstroem; Kumar; Heikkilae; Murzin, D.Yu.
Applied Catalysis A: General, 2011 , vol. 397, # 1-2 p. 13 - 21
反应条件
scandium tris(trifluoromethanesulfonate) T=20°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 43, # 5 p. 851 - 855
反应条件
water T=170°C; 3 h; Inert atmosphere;
参考文献
Hu, Xun; Li, Chun-Zhu
Green Chemistry, 2011 , vol. 13, # 7 p. 1676 - 1679
反应条件
water T=170°C; 3 h; Inert atmosphere;
参考文献
Green Chemistry, , vol. 13, # 7 p. 1676 - 1679
反应条件
diethylesilane; tris(pentafluorophenyl)-borane in dichloromethane-d2 18 h; Inert atmosphereGlovebox;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 6 p. 1646 - 1649
Angew. Chem., , vol. 126, # 6 p. 1672 - 1675,4
反应条件
1.1: 1H-imidazole / tetrahydrofuran / 0 °C 2.1: magnesium / tetrahydrofuran; ethylene dibromide / 2 h / |Reflux 2.2: 1 h / 20 °C 2.3: 5 h / 20 - 150 °C 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C View Scheme
参考文献
ScinoPharm Taiwan, LTD.; Henschke, Julian Paul; Lin, Chen-Wei; Wu, Ping-Yu; Hsiao, Chi-Nung; Liao, Jyh-Hsiung; Hsiao, Tsung-Yu
Patent: US2014/128595 A1, 2014 ;
