3,6-二甲氧基-4-菲醇合成路线 (共 12 条)
反应条件
hydrogenchloride; potassium hydroxide in water
1 h; Heating;
参考文献
Theuns, Hubert G.; Janssen, Richard H. A. M.; Biessels, Hubertus W. A.; Salemink, Cornelis A.
Phytochemistry (Elsevier), 1985 , vol. 24, # 1 p. 163 - 170
反应条件
chloroformic acid ethyl ester in toluene
2 h; Heating;
参考文献
Lee, Dong Ung; Wiegrebe, Wolfgang
Archiv der Pharmazie (Weinheim, Germany), 1986 , vol. 319, # 8 p. 694 - 704
反应条件
benzenethiol sodium salt in acetonitrile; butanone
8 h; Heating;
参考文献
Manoharan; Madyastha
Synthesis, 1983 , vol. No. 10, p. 809 - 812
反应条件
in acetonitrile; butanone
6 h; Heating;
参考文献
Manoharan; Madyastha
Synthesis, 1983 , vol. No. 10, p. 809 - 812
反应条件
in acetonitrile; butanone
1) 40 to 80 deg C, 2-3h, 2) 80 deg C, 8h;
参考文献
Manoharan, T. Samuel; Madyastha, K. Madhava; Singh, B. B.; Bhatnagar, S. P.; Weiss, Ulrich
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 1 p. 5 - 11
反应条件
lithium aluminium tetrahydride
Irradiation;
参考文献
Fleischhacker,W.; Vieboeck,F.
Monatshefte fuer Chemie, 1965 , vol. 96, # 5 p. 1512 - 1519
反应条件
in toluene
1 h; Ambient temperature;
参考文献
Lee, Dong Ung; Wiegrebe, Wolfgang
Archiv der Pharmazie (Weinheim, Germany), 1986 , vol. 319, # 8 p. 694 - 704
参考文献
Bertgen,C. et al.
Chemische Berichte, 1967 , vol. 100, p. 3002 - 3015
反应条件
in neat (no solvent)
T=100°C; 1 h; effect of additives; Product distributionMechanism;
参考文献
Allen, Andrew C.; Cooper, Donald A.; Moore, James M.; Teer, Charles B.
Journal of Organic Chemistry, 1984 , vol. 49, # 19 p. 3462 - 3465
参考文献
Knorr
Chemische Berichte, 1904 , vol. 37, p. 3501