1,1,3-三苯基-2-丙烯-1-醇合成路线 (共 16 条)
反应条件
cerium(III) chloride in tetrahydrofuran; diethyl ether; cyclohexane
T=-78°C; 0.5 h;
参考文献
Imamoto, Tsuneo; Takiyama, Noboyuki; Nakamura, Kimikazu; Hatajima, Toshihiko; Kamiya, Yasuo
Journal of the American Chemical Society, 1989 , vol. 111, # 12 p. 4392 - 4398
反应条件
1: With anhydrous iron chloride; potassium carbonate; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran
T=90°C; 22 h; Inert atmosphere;
2: With water; sodium chloride in tetrahydrofuran; ethyl acetate
Inert atmosphere;
参考文献
Zou, Tao; Pi, Sha-Sha; Li, Jin-Heng
Organic Letters, 2009 , vol. 11, # 2 p. 453 - 456
反应条件
cerium(III) chloride in tetrahydrofuran
T=0°C; 1 h;
参考文献
Imamoto, Tsuneo; Takiyama, Nobuyuki; Nakamura, Kamikazu
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4763 - 4766
反应条件
in tetrahydrofuran
Ambient temperature;
参考文献
Hou, Zhaomin; Fujiwara, Yuzo; Jintoku, Tetsuro; Mine, Norioki; Yokoo, Kazuhiro; Taniguchi, Hiroshi
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3524 - 3528
反应条件
potassium tert-butylate; oxygen; tert-butyl alcohol in dimethyl sulfoxide
参考文献
Barton,D.H.R.; Jones,D.W.
Journal of the Chemical Society, 1965 , p. 3563 - 3570
反应条件
diethyl ether
Zersetzung des Reaktionsprodukts mit Ammoniumchlorid-Loesung;
参考文献
Ziegler; Richter; Schnell
Justus Liebigs Annalen der Chemie, 1925 , vol. 443, p. 179
反应条件
ytterbium
1.) THF, -30 deg C, 1 h 35 min; 2.) THF, r.t., overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Yokoo, Kazuhiro; Yamanaka, Yasuhiro; Fukagawa, Toshihiro; Taniguchi, Hiroshi; Fujiwara, Yuzo
Chemistry Letters, 1983 , p. 1301 - 1302
反应条件
in tetrahydrofuran
T=-40°C; other PhLnI (Ln = Eu, Sm, Yb); Product distribution;
参考文献
Sigalov, A. B.; Rybakova, L. F.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, p. 1539
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 7 p. 1690
参考文献
Rozhkov,I.N.; Makin,S.M.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, # 1 p. 59 - 65,57 - 63
反应条件
in tetrahydrofuran
other α,β-unsaturated carbonyl compounds; var.temp., substrate ratios; Product distributionMechanism;
参考文献
Hou, Zhaomin; Fujiwara, Yuzo; Jintoku, Tetsuro; Mine, Norioki; Yokoo, Kazuhiro; Taniguchi, Hiroshi
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3524 - 3528