1,1'-氧基二(环己烷)合成路线 （共 57 条）
反应条件
hydrogen; nickel in 2-methyl cyclohexane
T=90°C; P=37503.8 Torr; 2.5 h; chemoselective reaction;
参考文献
Wang, Xingyu; Rinaldi, Roberto
ChemSusChem, 2012 , vol. 5, # 8 p. 1455 - 1466
反应条件
hydrogen; nickel in decalin
T=90°C; P=37503.8 Torr; 2.5 h; chemoselective reaction;
参考文献
Wang, Xingyu; Rinaldi, Roberto
ChemSusChem, 2012 , vol. 5, # 8 p. 1455 - 1466
反应条件
nickel
T=165 - 170°C; P=7600 - 11400 Torr; Hydrogenation;
参考文献
Schrauth; Wege
Chemische Berichte, 1924 , vol. 57, p. 858
反应条件
trimethyl-silane; trimethylsilyl iodide in dichloromethane
1.) 0 deg C, 60 min, 2.) room temperature, 8 h; further catalyst;
参考文献
Sassaman, Mark B.; Prakash, G. K. Surya; Olah, George A.
Tetrahedron, 1988 , vol. 44, # 13 p. 3771 - 3780
反应条件
hydrogen; platinum on activated charcoal in water
T=89.85 - 99.85°C; Dehalogenation; hydrogenation; P=760 Torr; 0.333333 h; microwave irradiation; Product distribution;
参考文献
Wada, Yuji; Yin, Hengbo; Kitamura, Takayuki; Yanagida, Shozo
Chemistry Letters, 2000 , # 6 p. 632 - 633
反应条件
hydrogen; 1 wtpercent K/1 wtpercent Pt/SiO2
T=425°C; P=3345.86 Torr; Product distribution / selectivity;
参考文献
EXXONMOBIL CHEMICAL PATENTS INC.; XU, Teng; DAKKA, Jihad, M.; BECKER, Christopher, L.; KUECHLER, Keith, H.; BENITEZ, Francisco, M.; SMITH, Charles, M.; NAIR, Hari
Patent: WO2011/96989 A1, 2011 ;
Location in patent: Page/Page column 23; 25 ;
反应条件
copper acetylacetonate; trichloromonobromomethane
T=150°C; 8 h; Inert atmosphereSealed tube;
参考文献
Khusnutdinov, R. I.; Bayguzina, A. R.; Gimaletdinova, L. I.; Dzhemilev, U. M.
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 9 p. 1191 - 1196,6
Zhurnal Organicheskoi Khimii, 2012 , vol. 48, # 9 p. 1191 - 1196,6
反应条件
hydrogen; platinum on activated charcoal in water
T=89.85 - 99.85°C; Dehalogenation; hydrogenation; P=760 Torr; 0.05 h; microwave irradiation; Product distribution; Further Variations:SolventsTemperatures;
参考文献
Wada, Yuji; Yin, Hengbo; Kitamura, Takayuki; Yanagida, Shozo
Chemistry Letters, 2000 , # 6 p. 632 - 633
反应条件
copper acetylacetonate; carbon tetrabromide
T=150°C; 8 h; Inert atmosphereSealed tube;
参考文献
Khusnutdinov, R. I.; Bayguzina, A. R.; Gimaletdinova, L. I.; Dzhemilev, U. M.
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 9 p. 1191 - 1196,6
Zhurnal Organicheskoi Khimii, 2012 , vol. 48, # 9 p. 1191 - 1196,6
反应条件
Montmorillonite K 10
6 h; Heating;
参考文献
Deshmukh; Gumaste; Bhawal
Synthetic Communications, 1995 , vol. 25, # 24 p. 3939 - 3944
