1,1'-氧基二(环己烷)合成路线 （共 57 条）
反应条件
1: With bromine in dichloromethane; water 1 h; Reflux; 2: With dihydrogen peroxide in dichloromethane; water 4 h; Reflux;
参考文献
Amati, Alessandro; Dosualdo, Gabriele; Zhao, Lihua; Bravo, Anna; Fontana, Francesca; Minisci, Francesco; Bjorsvik, Hans-Rene
Organic Process Research and Development, 1998 , vol. 2, # 4 p. 261 - 269
反应条件
hafnium(IV) trifluoromethanesulfonate; palladium 10 on activated carbon; hydrogen in neat (no solvent) T=150°C; P=30003 Torr; 3 h; Sealed tubeInert atmosphereGreen chemistry;
参考文献
Li, Zhi; Assary, Rajeev S.; Atesin, Abdurrahman C.; Curtiss, Larry A.; Marks, Tobin J.
Journal of the American Chemical Society, 2014 , vol. 136, # 1 p. 104 - 107
反应条件
phosphorus; hydrogen iodide T=200°C;
参考文献
Lacourt
Bulletin des Societes Chimiques Belges, 1927 , vol. 36, p. 348,350, 352
Chem. Zentralbl., 1927 , vol. 98, # II p. 923
参考文献
Lacourt
Bulletin des Societes Chimiques Belges, 1927 , vol. 36, p. 348,350, 352
Chem. Zentralbl., 1927 , vol. 98, # II p. 923
反应条件
aluminium silicate T=170°C;
反应条件
kieselguhr; nickel
T=150°C; P=117681 Torr; Hydrogenation;
参考文献
Komatsu; Masumoto
Bulletin of the Chemical Society of Japan, 1930 , vol. 5, p. 247
Chem. Zentralbl., 1930 , vol. 101, # II p. 2865
Full Text Show Details
Adkins; Cramer
Journal of the American Chemical Society, 1930 , vol. 52, p. 4349,4354
反应条件
1,1,3,3-tetramethyldisiloxane; copper(II) bis(trifluoromethanesulfonate) in dichloromethane
T=20°C; 1 h;
参考文献
Zhang, Yin-Jie; Dayoub, Wissam; Chen, Guo-Rong; Lemaire, Marc
Tetrahedron, 2012 , vol. 68, # 36 p. 7400 - 7407
反应条件
hydrogen; Rh on carbon in methanol
T=20°C; P=760.051 Torr; 2.5 h;
参考文献
Park, Kang Hyun; Jang, Kwonho; Kim, Hae Jin; Son, Seung Uk
Angewandte Chemie - International Edition, 2007 , vol. 46, # 7 p. 1152 - 1155
反应条件
triethylsilane; trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=-78 - -30°C;
参考文献
Hatakeyama, Susumi; Mori, Hisato; Kitano, Kaori; Yamada, Hidetoshi; Nishizawa, Mugio
Tetrahedron Letters, 1994 , vol. 35, # 25 p. 4367 - 4370
反应条件
chlorotris[3-[tris(ethoxy)silyl]propylisocyanide]rhodium complex; palladium matal-containing silica-supported catalyst in n-heptane
T=40°C; P=760 Torr; 22 h;
参考文献
Gao; Angelici
Journal of the American Chemical Society, 1997 , vol. 119, # 29 p. 6937 - 6938
