4-氨基-2,6-二甲基嘧啶合成路线 （共 38 条）
反应条件
magnesium T=120 - 130°C; 14 h;
参考文献
Burns, Timothy P.; Rieke, Reuben D.
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3674 - 3680
反应条件
ammonia; yttrium (III) trifluoromethanesulfonate T=-196 - 200°C; 24 h;
参考文献
Forsberg, John H.; Spaziano, Vincent T.; Klump, Stephen P.; Sanders, Kathleen M.
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 767 - 770
反应条件
tetreamethyl ammonium hydroxide T=80°C; 15.5 h;
参考文献
Smyrl, Norman R.; Smithwick, Robert W.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 493 - 496
反应条件
zinc(II) chloride in isopropyl alcohol; toluene T=90°C; 16 h; Inert atmosphere;
参考文献
Letinois, Ulla; Schuetz, Jan; Haerter, Ralph; Stoll, Rinke; Huffschmidt, Florian; Bonrath, Werner; Karge, Reinhard
Organic Process Research and Development, 2013 , vol. 17, # 3 p. 427 - 431
反应条件
yttrium (III) trifluoromethanesulfonate T=-196 - 200°C; 24 h;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1201658 A1, 2002 ;
Location in patent: Example 4 ;
反应条件
1: With Rhodium trichloride; borane-THF in tetrahydrofuran T=20°C; 1.5 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran T=0°C; 4 h; Further byproducts given;
参考文献
Buranov, Anvar U.; Morrill, Terence C.
Tetrahedron Letters, 2003 , vol. 44, # 33 p. 6301 - 6304
反应条件
tetreamethyl ammonium hydroxide T=120°C; 24 h;
参考文献
Smyrl, Norman R.; Smithwick, Robert W.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 493 - 496
反应条件
ethanol; ammonia T=150°C;
参考文献
Schmidt
Chemische Berichte, 1902 , vol. 35, p. 1577
反应条件
T=150°C; P=6251820 Torr;
参考文献
Cairns et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 5633,5635
反应条件
(Ph3Ge)3GeNMe2; triphenylgermanium hydride T=90°C; 72 h; Inert atmosphere;
参考文献
Samanamu, Christian R.; Amadoruge, Monika L.; Yoder, Claude H.; Golen, James A.; Moore, Curtis E.; Rheingold, Arnold L.; Materer, Nicholas F.; Weinert, Charles S.
Organometallics, 2011 , vol. 30, # 5 p. 1046 - 1058
