六氢-1,3,5-三嗪-1,3,5-三(乙腈)合成路线 (共 11 条)
反应条件
Montmorillonite K10 in acetonitrile T=180°C; 0.5 h;
参考文献
Meierhenrich, Uwe J.; Munoz Caro, Guillermo M.; Schutte, Willem A.; Thiemann, Wolfram H.-P.; Barbier, Bernard; Brack, Andre
Chemistry - A European Journal, 2005 , vol. 11, # 17 p. 4895 - 4900
反应条件
T=190°C; Yield given;
参考文献
Dammel, Ralph; Bock, Hans
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 7 p. 810 - 814
反应条件
3 A molecular sieve T=220°C; P=0.1 Torr; flash vaccum pyrolysis at variation of temp.; Product distribution;
参考文献
Helvetica Chimica Acta, , vol. 77, # 8 p. 2209 - 2250
反应条件
hydrogenchloride; phosphorous acid trimethyl ester in toluene
参考文献
Stauffer Chemical Company
Patent: US4427599 A1, 1984 ;
反应条件
ammonium chloride in water
参考文献
Dammel, Ralph; Bock, Hans
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 7 p. 810 - 814
参考文献
Monsanto Company
Patent: US4083898 A1, 1978 ;
反应条件
in chloroform; acetonitrile
参考文献
Monsanto Company
Patent: US4089671 A1, 1978 ;
反应条件
1: HNO3, Ac2O / 10 - 15 °C
2: aq. HCl
View Scheme
参考文献
Denkstein,J.; Kaderabek,V.
Collection of Czechoslovak Chemical Communications, 1966 , vol. 31, p. 2928 - 2937
反应条件
1: HNO3, Ac2O, NH4NO3 / 60 - 65 °C
2: aq. HCl
View Scheme
参考文献
Denkstein,J.; Kaderabek,V.
Collection of Czechoslovak Chemical Communications, 1966 , vol. 31, p. 2928 - 2937
反应条件
potassium hydroxide
und Erwaermen des Reaktionsprodukts mit wss.HCl;
参考文献
Mahajani; Ray
Journal of the Indian Chemical Society, 1956 , vol. 33, p. 455,457