[CpTiCl(NP-t-Bu3)(C4H8)] in deuterated toluene
T=110°C; 216 h;
参考文献
Masuda, Jason D.; Hoskin, Aaron J.; Graham, Todd W.; Beddie, Chad; Fermin, Maria C.; Etkin, Nola; Stephan, Douglas W.
Chemistry - A European Journal, 2006 , vol. 12, # 34 p. 8696 - 8707
in toluene
Ar atmosphere, stirring (60°C, 3 h); solvent removal (14 Torr), B-product isolated by sublimation (30-40°C, 0.001 Torr); byproducts identified by MS and (31)P-NMR;
Reesor; Wright
Journal of Organic Chemistry, 1957 , vol. 22, p. 375,380
Full Text Show Details
Weil et al.
Helvetica Chimica Acta, 1952 , vol. 35, p. 616