1,2-二甲基-1,1,2,2-四氯二硅烷合成路线 (共 60 条)
参考文献
Watanabe, Hamao; Inose, Jun; Fukushima, Koji; Kougo, Yuichi; Nagai, Yoichiro
Chemistry Letters, 1983 , p. 1711 - 1714
参考文献
Watanabe, Hamao; Inose, Jun; Fukushima, Koji; Kougo, Yuichi; Nagai, Yoichiro
Chemistry Letters, 1983 , p. 1711 - 1714
参考文献
Watanabe, Hamao; Inose, Jun; Fukushima, Koji; Kougo, Yuichi; Nagai, Yoichiro
Chemistry Letters, 1983 , p. 1711 - 1714
反应条件
1.1.2.2-tetrabromodimethyldisilane in benzene-d6
T=60°C; 10 h; other times, Cl-Br-exchange; Product distribution;
参考文献
Schmoelzer, Harald; Hengge, Edwin
Monatshefte fuer Chemie, 1984 , vol. 115, p. 1125 - 1132
反应条件
aluminium trichloride in benzene-d6; benzene
T=90°C; 1 h; no reaction in the absence of catalyst; Product distribution;
参考文献
Schmoelzer, H.; Hengge, E.
Journal of Organometallic Chemistry, 1984 , vol. 260, # 1 p. 31 - 40
反应条件
tri-n-butyl-tin hydride in toluene
48 h; Ambient temperatureother chlorodisilanes; Product distribution;
参考文献
Herzog, U.; Roewer, G.; Paetzold, U.
Journal of Organometallic Chemistry, 1995 , vol. 494, # 12 p. 143 - 148
反应条件
ZnF2 in 1,1,2,3,4,4-hexachloro-1,3-butadiene
参考文献
Schmoelzer, Harald; Hengge, Edwin
Monatshefte fuer Chemie, 1984 , vol. 115, p. 1125 - 1132
反应条件
in diethyl ether
Ambient temperature;
参考文献
Hengge, Edwin; Kalchauer, Wilfried
Monatshefte fuer Chemie, 1990 , vol. 121, # 10 p. 793 - 802
参考文献
Barton,T.J.; Banasiak,D.S.
Journal of the American Chemical Society, 1977 , vol. 99, p. 5199 - 5200
反应条件
hydrogenchloride
T=430 - 750°C; 72 h; Conversion of starting material;
参考文献
Wacker-Chemie GmbH
Patent: US2005/113591 A1, 2005 ;
Location in patent: Page/Page column 2 ;