1,2-二甲基-1,1,2,2-四氯二硅烷合成路线 (共 60 条)
反应条件
aluminium trichloride; acetyl chloride T=125°C; 1 h;
参考文献
Grobe, Joseph; Henkel, Gerald; Krebs, Bernt; Voulgarakis, Nikolaos
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1984 , vol. 39, # 3 p. 341 - 351
反应条件
aluminium trichloride; acetyl chloride T=115°C;
参考文献
Knopf; Herzog; Roewer; Brendler; Rheinwald; Lang
Journal of Organometallic Chemistry, 2002 , vol. 662, # 1-2 p. 14 - 22
反应条件
hydrogenchloride; aluminium trichloride in benzene
参考文献
Ernst, Margot; Schenzel, Karla; Jaehn, Anke; Hassler, Karl
Journal of Molecular Structure, 1997 , vol. 412, # 1-2 p. 83 - 95
反应条件
aluminium trichloride; acetyl chloride T=125°C; Title compound not separated from byproducts;
参考文献
Knopf; Herzog; Roewer; Brendler; Rheinwald; Lang
Journal of Organometallic Chemistry, 2002 , vol. 662, # 1-2 p. 14 - 22
反应条件
aluminium trichloride; acetyl chloride
参考文献
Sakurai,H. et al.
Journal of Organometallic Chemistry, 1967 , vol. 7, p. P15 - P16
反应条件
Si2Cl6; aluminium trichloride in benzene-d6 T=200°C; 120 h; var. temp.; Product distribution;
参考文献
Schmoelzer, H.; Hengge, E.
Journal of Organometallic Chemistry, 1984 , vol. 260, # 1 p. 31 - 40
反应条件
n-butyllithium 1.) diethyl ether, hexane, RT, 1h, 2.) diethyl ether, hexane, 0 - 20 deg C, 1 h; Multistep reaction;
参考文献
Tinga, Markus A. G. M.; Buisman, Godfried J. H.; Schat, Gerrit; Akkerman, Otto S.; Bickelhaupt, Friedrich; et al.
Journal of Organometallic Chemistry, 1994 , vol. 484, # 1-2 p. 137 - 146
反应条件
ammonia in diethyl ether
参考文献
Maier, G.; Reisenauer, H. P.; Schoettler, K.; Wessolek-Kraus, U.
Journal of Organometallic Chemistry, 1989 , vol. 366, p. 25 - 38
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C;
参考文献
Matsumoto, Hideyuki; Kasahara, Miyuki; Matsubara, Ikuya; Takahashi, Masatoshi; Arai, Takeshi; et al.
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 99 - 108
参考文献
Wacker-Chemie GmbH
Patent: US5268496 A1, 1993 ;