2-氯-2-苯基苯乙酮合成路线 （共 108 条）
反应条件
pyridine; tert.-butylhydroperoxide; TiCl2(OPri)2; 3 A molecular sieve 1) THF, CH2Cl2, r.t., 45 min, 2) THF, CH2Cl2, -50 deg C, 1 h, r.t., 12 h; Yield givenMultistep reaction;
参考文献
Krohn, Karsten; Steingroever, Klaus; Vinke, Ingeborg
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 1999 , vol. 341, # 1 p. 62 - 64
参考文献
Buck; Ide
Journal of the American Chemical Society, 1932 , vol. 54, p. 4359,4364
参考文献
Schroeter
Chemische Berichte, 1909 , vol. 42, p. 2346
Chem. Zentralbl., 1910 , vol. 81, # I p. 1470
参考文献
Mc Kenzie; Wren
Journal of the Chemical Society, 1910 , vol. 97, p. 481
参考文献
Curtius; Lang
Journal fuer Praktische Chemie (Leipzig), 1891 , vol. <2> 44, p. 564
参考文献
Ward
Journal of the Chemical Society, 1929 , p. 1549
Organic Syntheses, 1932 , vol. 12, p. 20
反应条件
1: 1.) K2CO3 / 1.) CHCl3, 1 h, 2.) 24 h 2: 70 percent / glacial acetic acid / 12 h / Heating View Scheme
参考文献
Padmanabhan, P. V.; Ramana, D. V.; Ramadas, S. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 957 - 958
参考文献
Ochiai et al.
Yakugaku Zasshi, 1939 , vol. 59, p. 462,468; dtsch. Ref. S. 228, 233
Chem.Abstr., 1954 , p. 0 5449
反应条件
(i) P2S5, dioxane, (ii) /BRN= 744474/; Multistep reaction;
参考文献
Vernin,G. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 4523 - 4533
参考文献
Dauben et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 2082
