反应条件
1.1: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 1 h / 0 - 10 °C / Large scale reaction
1.2: 3 h / 0 - 10 °C / Large scale reaction
2.1: methanol / 16.5 h / 20 °C / Large scale reaction
View Scheme
参考文献
Sawai, Yasuhiro; Yamane, Taihei; Ikeuchi, Motoki; Kawaguchi, Shinji; Yamada, Masatoshi; Yamano, Mitsuhisa
Organic Process Research and Development, 2010 , vol. 14, # 5 p. 1110 - 1117