2-庚基-1,3-二氧戊环合成路线 （共 19 条）
反应条件
indium(III) chloride in methanol; water 1.33333 h; Heating;
参考文献
Ranu, Brindaban C.; Jana, Ranjan; Samanta, Sampak
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 4 p. 446 - 450
反应条件
oxygen; zinc(II) chloride; CoCl2 in ethylene glycol dimethyl ether T=90°C; 30 h;
参考文献
Canadian Journal of Chemistry, , vol. 71, # 1 p. 84 - 89
反应条件
oxygen; zinc(II) chloride; CoCl2 in ethylene glycol dimethyl ether T=90°C; 30 h;
参考文献
Canadian Journal of Chemistry, , vol. 71, # 1 p. 84 - 89
反应条件
trimethylsilyl trifluoromethanesulfonate in tetrahydrofuran T=-78 - 0°C;
参考文献
Hunter, Roger; Michael, Joseph P.; Tomlinson, Geoffrey D.
Tetrahedron, 1994 , vol. 50, # 3 p. 871 - 888
反应条件
1: 56 percent / tetrabutylammonium bromide, Br2, ethylene glycol / CH2Cl2 / 0.5 h 2: KOH / methanol / 10 h / Heating 3: p-toluenesulfonic acid, H2O / 4 h / Ambient temperature View Scheme
参考文献
Vasil'ev, A. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 6.1 p. 876 - 880
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 6 p. 822 - 826
反应条件
hydrogenchloride; hydroxylamine hydrochloride 2 h; Heating;
参考文献
Yamauchi
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 11 p. 2042 - 2043
反应条件
hydroxylamine hydrochloride; toluene-4-sulfonic acid in ethanol 2 h; Heatingother aliphatic and aromatic acetals; without addition of TsOH and with HCl; MechanismProduct distribution;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 41, # 11 p. 2042 - 2043
参考文献
Rosenthal,I.; Elad,D.
Journal of Organic Chemistry, 1968 , vol. 33, p. 805 - 811
反应条件
Envirocat EPZG supported reagent
0.0333333 h; microwave irradiation;
参考文献
Beregszaszi, Timea; Molnar, Arpad
Synthetic Communications, 1997 , vol. 27, # 21 p. 3705 - 3709
反应条件
lithium chloride; copper dichloride in tetrahydrofuran
T=-10°C;
参考文献
Volkmann, Robert A.; Davis, Jeffery T.; Meltz, Clifford N.
Journal of Organic Chemistry, 1983 , vol. 48, # 10 p. 1767 - 1769
