(3,3-二甲基-1-丁炔)-苯合成路线 (共 61 条)
反应条件
water; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile Heating;
参考文献
Zupan, Marko; Iskra, Jernej; Stavber, Stojan
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 259 - 260
反应条件
methanol; calcium sulfate 1 h; Ambient temperature;
参考文献
Stavber, Stojan; Zupan, Marko
Journal of Organic Chemistry, 1987 , vol. 52, # 22 p. 5022 - 5025
反应条件
calcium sulfate 1 h; Ambient temperature;
参考文献
Stavber, Stojan; Zupan, Marko
Journal of Organic Chemistry, 1987 , vol. 52, # 22 p. 5022 - 5025
反应条件
di-tert-butyl peroxide in benzene T=150°C; 3 h; Yields of byproduct given;
参考文献
Benati, Luisa; Montevecchi, Pier Carlo; Spagnolo, Piero
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 13 p. 1659 - 1664
反应条件
(i) toluene, (ii) H2O; Multistep reaction;
参考文献
Eisch,J.J.; Amtmann,R.
Journal of Organic Chemistry, 1972 , vol. 37, p. 3410 - 3415
反应条件
1: carbon monoxide; phenyl-tert-butylacetylene; N-(ethoxycarbonyl)-2-iodoaniline With pyridine; palladium diacetate; tetrabutyl-ammonium chloride in N,N-dimethyl-formamide T=100°C; P=760 Torr; 12 h; 2: ethanol With sodium hydroxide T=20°C; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 20 p. 6772 - 6780
反应条件
1: With titanium tetrachloride; tert-butylamine; aniline in toluene T=150°C; 22 h; 2: With water; silica gel in dichloromethane; toluene T=20°C; Further stages.;
参考文献
Kim, Hye Ryung; Yun, Jaesook
Chemical Communications, 2011 , vol. 47, # 10 p. 2943 - 2945
反应条件
aluminum oxide; phosphorus(III) iodide in dichloromethane 36 h;
参考文献
Kropp, Paul J.; Crawford, Scott D.
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3102 - 3112
反应条件
thionyl chloride; silica gel in dichloromethane 3 h; various reaction times and adsorbent; Product distribution;
参考文献
Kropp, Paul J.; Crawford, Scott D.
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3102 - 3112
反应条件
silica gel; phosphorus tribromide in dichloromethane 0.3 h; various reaction times and adsorbent; Product distribution;
参考文献
Kropp, Paul J.; Crawford, Scott D.
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3102 - 3112