2-羟基-1,2,2-三苯乙酮合成路线 (共 78 条)
反应条件
oxygen in benzene T=20°C; 2 h; Irradiationpresence of α-methylstyrene, other solvent; Product distributionQuantum yield;
参考文献
Journal of the American Chemical Society, , vol. 103, # 8 p. 2049 - 2053
参考文献
Blatt; Barnes
Journal of the American Chemical Society, 1934 , vol. 56, p. 1148,1150
反应条件
in acetonitrile T=20°C; Irradiation; KineticsQuantum yield;
参考文献
Baumann, Harald; Timpe, Hans-Joachim
Zeitschrift fuer Chemie (Stuttgart, Germany), 1984 , vol. 24, # 1 p. 19 - 20
参考文献
Acree
Chemische Berichte, 1904 , vol. 37, p. 2762
American Chemical Journal, 1905 , vol. 33, p. 189
反应条件
1: 58 percent / TFA (trifluoromethanesulphonic acid) / 1,2-dichloro-ethane / 0.33 h / 100 °C / in a sealed tube 2: 15 percent / dibenzoyl peroxide, trifluoroacetic acid (TFA) / 1,2-dichloro-ethane / 24 h / 50 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1987 - 1996
反应条件
Irradiationwith a 2-methoxy-2H-pyrane as proptnic acid indicator; Quantum yield;
参考文献
Zeitschrift fuer Chemie (Stuttgart, Germany), , vol. 24, # 8 p. 287 - 288
反应条件
2: 240 - 250 °C 3: LiAlH4 / tetrahydrofuran View Scheme
参考文献
Hofmann,H. et al.
Chemische Berichte, 1971 , vol. 104, p. 2134 - 2142
反应条件
1: sodium amalgam; alcohol 2: bei der trocknen Destillation View Scheme
参考文献
Chem. Zentralbl., , vol. 68, # II p. 662
参考文献
Journal of the American Chemical Society, , vol. 74, p. 5643,5645
反应条件
1: in tetrahydrofuran
T=0 - 20°C; 24 h; Inert atmosphere;
2: With ammonium chloride in tetrahydrofuran
Saturated solution;
参考文献
Abualhasan, Murad N.; Good, James A.D.; Wittayanarakul, Kitiyaporn; Anthony, Nahoum G.; Berretta, Giacomo; Rath, Oliver; Kozielski, Frank; Sutcliffe, Oliver B.; MacKay, Simon P.
European Journal of Medicinal Chemistry, 2012 , vol. 54, p. 483 - 498