2,2-二甲基-3-己醇合成路线 （共 35 条）
反应条件
titanium(IV) isopropylate in tetrahydrofuran T=-78 - 0°C;
参考文献
Kulinkovich, Oleg G.; Kananovich, Dzmitry G.
European Journal of Organic Chemistry, 2007 , # 13 p. 2121 - 2132
反应条件
1: in diethyl ether; pentane T=-78 - 20°C; 3.5 h; Inert atmosphere; 2: With water; ammonium chloride in diethyl ether; pentane
参考文献
Mello, Rossella; Martinez-Ferrer, Jaime; Alcalde-Aragones, Ana; Varea, Teresa; Acerete, Rafael; Gonzalez-Nunez, Maria Elena; Asensio, Gregorio
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 10129 - 10139
反应条件
in diethyl ether; pentane 1.) -78 deg C, 1h, 2.) room temp., 2.5 h;
参考文献
Heathcock, , Clayton H.; Lampe, John
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4330 - 4337
参考文献
Yamamura, Tomoya; Nakatsuka, Hiroshi; Tanaka, Shinji; Kitamura, Masato
Angewandte Chemie - International Edition, 2013 , vol. 52, # 35 p. 9313 - 9315
Angew. Chem., 2013 , vol. 125, # 35 p. 9483 - 9485
参考文献
Whitmore
Recueil des Travaux Chimiques des Pays-Bas, 1938 , vol. 57, p. 566
Full Text Show Details
Greenwood; Whitmore; Crooks
Journal of the American Chemical Society, 1938 , vol. 60, p. 2028
反应条件
1: copper / 250 - 300 °C 2: diethyl ether View Scheme
参考文献
Conant; Webb; Mendum
Journal of the American Chemical Society, 1929 , vol. 51, p. 1253
参考文献
Whitmore et al.
Journal of the American Chemical Society, 1938 , vol. 60, p. 2459,2788,63<1941>647
Recueil des Travaux Chimiques des Pays-Bas, 1938 , vol. 57, p. 567
参考文献
Conant; Webb; Mendum
Journal of the American Chemical Society, 1929 , vol. 51, p. 1253
参考文献
Conant; Webb; Mendum
Journal of the American Chemical Society, 1929 , vol. 51, p. 1253
反应条件
1: diethyl ether; sodium amide / nachfolgendes Behandeln mit Aethyljodid 2: sodium; alcohol View Scheme
参考文献
Haller; Bauer
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1910 , vol. 150, p. 588
Annales de Chimie (Cachan, France), 1913 , vol. <8>29, p. 330
