1-(4-溴丁基)-4-乙烯基苯合成路线 （共 3 条）
反应条件
1: 1-(Chloromethyl)-4-vinylbenzene With iodine; magnesium in diethyl ether
T=0 - 20°C; 4.5 h;
2: 1,3-dibromo-propane With dilithium tetrachlorocuprate in tetrahydrofuran; diethyl ether
T=0 - 20°C; Further stages.;
参考文献
Seki, Atsushi; Ishiwata, Fusae; Takizawa, Youichi; Asami, Masatoshi
Tetrahedron, 2004 , vol. 60, # 23 p. 5001 - 5011
反应条件
Br2Cu(1-)*Li(1+) in tetrahydrofuran
T=20°C; 5 h;
参考文献
Bertini, Vincenzo; Alfei, Silvana; Pocci, Marco; Lucchesini, Francesco; Picci, Nevio; Iemma, Francesca
Tetrahedron, 2004 , vol. 60, # 50 p. 11407 - 11414
反应条件
in N,N-dimethyl-formamide
T=55°C; 17 h;
参考文献
Bertini, Vincenzo; Alfei, Silvana; Pocci, Marco; Lucchesini, Francesco; Picci, Nevio; Iemma, Francesca
Tetrahedron, 2004 , vol. 60, # 50 p. 11407 - 11414
