1-(2-甲基苯基)吡咯烷合成路线 (共 11 条)
反应条件
potassium carbonate in ethanol; water
T=120°C; P=3878.71 Torr; 0.0833333 h;
参考文献
He, Hongjie; Lin, Qi; Liu, Xiaofeng; Yang, Yongtai; Zhou, Yaming; Jia, Yu; Gao, Xiang
Synthetic Communications, 2012 , vol. 42, # 17 p. 2512 - 2525
反应条件
triethylamine; dichloro bis(acetonitrile) palladium(II) in acetonitrile
T=20°C; 2 h;
参考文献
Ishikawa; Uedo; Tani; Saito
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 186 - 191
反应条件
hydrogen; 1,4-di(diphenylphosphino)-butane; η6-C6H6BPh3-Rh(COD)+
T=80°C; P=26220 Torr;
参考文献
Zhou, Jian-Qiang; Alper, Howard
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3328 - 3331
反应条件
styrene; [2,2']bipyridinyl; sodium tert-pentoxide; sodium hydride; nickel in tetrahydrofuran
Condensation; 4 h; Heating; Product distribution; Further Variations:other reaction time, various contents of Ni(0);
参考文献
Krinsky, Jamin L.; Martinez, Alberto; Godard, Cyril; Castillon, Sergio; Claver, Carmen
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 460 - 474
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol
T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79
反应条件
aluminum oxide
T=320°C;
参考文献
Walkup, Robert E.; Searles, Scott
Tetrahedron, 1985 , vol. 41, # 1 p. 101 - 106
反应条件
potassium hydroxide; pentacarbonyliron(0); carbon monoxide in ethanol; water
18 h; Ambient temperature;
参考文献
Shim, Sang Chul; Huh, Keun Tai; Park, Woo Hiun
Tetrahedron, 1986 , vol. 42, # 1 p. 259 - 264
反应条件
styrene; [2,2']bipyridinyl; nickel diacetate; sodium tert-pentoxide; sodium hydride in tetrahydrofuran
3 h;
参考文献
Brenner, Eric; Fort, Yves
Tetrahedron Letters, 1998 , vol. 39, # 30 p. 5359 - 5362
反应条件
aluminum oxide
T=300°C;
参考文献
Walkup, Robert E.; Searles, Scott
Tetrahedron, 1985 , vol. 41, # 1 p. 101 - 106
反应条件
lithium aluminium tetrahydride
参考文献
Baddeley et al.
Journal of the Chemical Society, 1956 , p. 448