1-(苯磺酰)-1H-苯并三唑合成路线 （共 13 条）
反应条件
1-methyl-1H-imidazole in tetrahydrofuran 3 h; Heating;
参考文献
Katritzky; Zhang; Wu
Synthetic Communications, 1994 , vol. 24, # 2 p. 205 - 216
反应条件
1-methyl-1H-imidazole in toluene 30 h; Heating;
参考文献
Synthetic Communications, , vol. 24, # 2 p. 205 - 216
反应条件
1: acetonitrile With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: 1-(benzenesulphonyl)benzotriazole in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Katritzky, Alan R.; Abdel-Fattah, Ashraf A. A.; Vakulenko, Anatoliy V.; Tao, Hui
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9191 - 9197
反应条件
1: 2-picoline With lithium diisopropyl amide in tetrahydrofuran; n-heptane; ethylbenzene T=-78°C; 2: 1-(benzenesulphonyl)benzotriazole in tetrahydrofuran; n-heptane; ethylbenzene T=-78 - 20°C;
参考文献
Katritzky, Alan R.; Abdel-Fattah, Ashraf A. A.; Vakulenko, Anatoliy V.; Tao, Hui
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9191 - 9197
反应条件
1-methyl-1H-imidazole in xylene 13 h; Heating;
参考文献
Katritzky; Zhang; Wu
Synthetic Communications, 1994 , vol. 24, # 2 p. 205 - 216
反应条件
1-methyl-1H-imidazole in tetrahydrofuran 72 h; Heating;
参考文献
Katritzky; Zhang; Wu
Synthetic Communications, 1994 , vol. 24, # 2 p. 205 - 216
反应条件
silica gel
T=20°C; 3 h; Green chemistry; chemoselective reaction;
参考文献
Ghosh, Pranab; Mandal, Amitava
Journal of the Indian Chemical Society, 2012 , vol. 89, # 2 p. 261 - 268
参考文献
Katritzky, Alan R.; Shobana; Pernak, Juliusz; Afridi; Fan, Wei-Qiang
Tetrahedron, 1992 , vol. 48, # 37 p. 7817 - 7822
反应条件
hydrogenchloride; sodium nitrite
参考文献
Morgan; Micklethwait
Journal of the Chemical Society, 1905 , vol. 87, p. 80
反应条件
1: iron; diluted acetic acid
2: acetic acid; sodium nitrite
View Scheme
参考文献
Morgan; Micklethwait
Journal of the Chemical Society, 1905 , vol. 87, p. 80
