1-叠氮基-2,4-二硝基苯合成路线 (共 23 条)
参考文献
Gmelin Handbook: K: MVol.2, 1.2, page 248 - 251
反应条件
1: acetic acid 2: (EtO)3P / ethanol View Scheme
参考文献
Ghosh,P.B.; Whitehouse,M.W.
Journal of Medicinal Chemistry, 1968 , vol. 11, # 2 p. 305 - 311
反应条件
ammonia T=25°C; Kinetics;
参考文献
Ji, Pengju; Atherton, John H.; Page, Michael I.
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3286 - 3295
参考文献
Noelting; Grandmougin; Michel
Chemische Berichte, 1892 , vol. 25, p. 3338
反应条件
2: nitric acid / Faellen mit Wasser View Scheme
参考文献
Drost
Justus Liebigs Annalen der Chemie, 1899 , vol. 307, p. 49
反应条件
tetrabutylammonium halide in chlorobenzene T=60°C; 24 h;
参考文献
Landini, Dario; Maia, Angelamaria; Montanari, Fernando
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 461 - 466
反应条件
dinitrogen tetraoxide in tetrachloromethane; acetonitrile
T=-30°C; 0.166667 h;
参考文献
Kim, Yong Hae; Kim, Kweon; Shim, Sung Bo
Tetrahedron Letters, 1986 , vol. 27, # 39 p. 4749 - 4752
反应条件
sodium azide; benzyl-tri-(n-butyl)-ammonium bromide in 1,2-dichloro-ethane
T=29°C; 6 h;
参考文献
Lopez-Vidal, Eva M.; Fernandez-Mato, Antonio; Garcia, Marcos D.; Perez-Lorenzo, Moises; Peinador, Carlos; Quintela, Jose M.
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1265 - 1270
反应条件
sodium azide in acetonitrile
T=20°C; 20 h;
参考文献
Zaitsev; Vatsadze; Dalinger; Kachala; Nelyubina; Shevelev
Russian Chemical Bulletin, 2009 , vol. 58, # 10 p. 2109 - 2117
反应条件
oxygen; nitrogen(II) oxide in tetrahydrofuran
3 h; Ambient temperature;
参考文献
Matsuya, Yuji; Itoh, Takashi; Nagata, Kazuhiro; Ohsawa, Akio
Tetrahedron, 1997 , vol. 53, # 46 p. 15701 - 15710