3-苯基-1-(2-噻吩)-2-丙烯-1-酮合成路线 (共 10 条)
反应条件
potassium hydroxide in ethanol 24 h;
参考文献
Liu, Bin; Bao, Yinyin; Du, Fanfan; Wang, Hu; Tian, Jiao; Bai, Ruke
Chemical Communications, 2011 , vol. 47, # 6 p. 1731 - 1733
反应条件
zinc oxide T=25 - 30°C; Friedel-Crafts Acylation; 0.166667 h; regioselective reaction;
参考文献
More, Parmeshwar E.; Bandgar, Babasaheb P.; Kamble, Vinod T.
Catalysis Communications, 2012 , vol. 27, p. 30 - 32
反应条件
1: With potassium tert-butylate in tetrahydrofuran T=-78°C; 0.166667 h; 2: With sulfuric acid in ethylene glycol dimethyl ether T=-78°C; 0.166667 h;
参考文献
Yoshizawa, Kazuhiro; Shioiri, Takayuki
Tetrahedron Letters, 2006 , vol. 47, # 28 p. 4943 - 4945
反应条件
potassium hydroxide in ethanol T=20°C; 15 h;
参考文献
Katritzky, Alan R.; Rezende, Marcos C.
Journal of Chemical Research, Miniprint, 1980 , # 9 p. 4041 - 4056
反应条件
iron(III) chloride in carbon disulfide 3 h; Ambient temperature;
参考文献
El-Khagawa, Ahmed M.; El-Zohry, Maher F.; Ismail, Mohamed T.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 33, p. 25 - 32
反应条件
aluminium trichloride; nitromethane in carbon disulfide 3 h; Ambient temperature;
参考文献
El-Khagawa, Ahmed M.; El-Zohry, Maher F.; Ismail, Mohamed T.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 33, p. 25 - 32
反应条件
aluminium trichloride in carbon disulfide 3 h; Ambient temperatureother catalyst; Product distribution;
参考文献
El-Khagawa, Ahmed M.; El-Zohry, Maher F.; Ismail, Mohamed T.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 33, p. 25 - 32
参考文献
Brunswig
Chemische Berichte, 1886 , vol. 19, p. 2893
反应条件
triethylamine in ethanol Condensation; 8 h; Heating;
参考文献
Attaby, Fawzy A.
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 139, p. 1 - 12
反应条件
hydrazine monohydrochloride in N,N-dimethyl-formamide
2 h; Reflux;
参考文献
Ingle; Doshi; Raut
Oriental Journal of Chemistry, 2010 , vol. 26, # 4 p. 1517 - 1520