2-氧代-2,3-二氢-1H-咪唑-4-羧酸合成路线 (共 7 条)
反应条件
sodium carbonate; silver(l) oxide in water T=70°C; 2 h; in a sealed tube;
参考文献
Uramoto; Kobinata; Isono; et al.
Tetrahedron, 1982 , vol. 38, # 11 p. 1599 - 1608
反应条件
sulfuric acid; sulfur trioxide anschliessend mit Harnstoff;
参考文献
Hilbert
Journal of the American Chemical Society, 1932 , vol. 54, p. 3413,3417
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Nakajima
Nagasaki med. J.Chem.Abstr., 1958 , vol. 33, p. 825,826
Nagasaki med. J.Chem.Abstr., 1958 , p. 18591
反应条件
sulfuric acid T=80°C; 1 h;
参考文献
Baxter, Robert L.; Camp, Dominic J.; Coutts, Andrew; Shaw, Nicholas
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 2 p. 255 - 258
反应条件
potassium carbonate 4 h; Heating;
参考文献
Baxter, Robert L.; Camp, Dominic J.; Coutts, Andrew; Shaw, Nicholas
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 2 p. 255 - 258
反应条件
nickel; sodium carbonate T=100°C; P=113268 Torr; Hydrogenation;
参考文献
Dittmer; Ferger; du Vigneaud
Journal of Biological Chemistry, 1946 , vol. 164, p. 26
参考文献
Hilbert
Journal of the American Chemical Society, 1932 , vol. 54, p. 3413,3417
反应条件
thionyl chloride
Heating;
参考文献
Dransfield, Paul J.; Dilley, Anja S.; Wang, Shaohui; Romo, Daniel
Tetrahedron, 2006 , vol. 62, # 22 p. 5223 - 5247