2,2-二甲基-1-苯基-1-丙醇合成路线 (共 26 条)
反应条件
potassium cyanide; sulfuric acid in anhydrous butyl ether T=60 - 80°C;
参考文献
Christol,H. et al.
Bulletin de la Societe Chimique de France, 1961 , p. 2319 - 2324
反应条件
iodosylbenzene; N,N'-bis(3,5-dichlorosalicylidene)-1,2-ethylenediamino-MnCl in acetonitrile T=20°C; 2 h;
参考文献
Synthetic Communications, , vol. 33, # 22 p. 3961 - 3967
反应条件
C10H16NO5; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=0°C; 6 h; Resolution of racemate;
参考文献
Tetrahedron Letters, , vol. 55, # 11 p. 1943 - 1945
反应条件
Titanium(IV) oxide; silver sulphate in acetonitrile Oxidation; elimination; 3 h; Irradiation;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 2 p. 311 - 315
反应条件
C10H16NO5; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=20°C;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 31 p. 8093 - 8097
Angew. Chem., , vol. 125, # 31 p. 8251 - 8255,5
反应条件
C10H16NO5; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=20°C;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 31 p. 8093 - 8097
Angew. Chem., , vol. 125, # 31 p. 8251 - 8255,5
反应条件
C10H16NO5; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=20°C;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 31 p. 8093 - 8097
Angew. Chem., , vol. 125, # 31 p. 8251 - 8255,5
反应条件
T=25 - 30°C; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 72, p. 4617
反应条件
T=28°C; Product distribution;
参考文献
Chemistry and Industry (London, United Kingdom), , p. 1451
反应条件
(R)-(+)-N-methylbenzoguanidine; trimethylacetic anhydride in diethyl ether T=20°C; 12 h; Resolution of racemate; optical yield given as percent ee;
参考文献
Nakata, Kenya; Shiina, Isamu
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 7092 - 7096