3-溴-1-三甲基硅基-1-丙炔合成路线 （共 36 条）
反应条件
phosphorus tribromide T=-5 - 20°C; Inert atmosphere;
参考文献
Inack Ngi, Samuel; Cherry, Khalil; Heran, Virginie; Commeiras, Laurent; Parrain, Jean-Luc; Duchene, Alain; Abarbri, Mohamed; Thibonnet, Jerome
Chemistry - A European Journal, 2011 , vol. 17, # 49 p. 13692 - 13696
反应条件
bromine; triphenylphosphine in dichloromethane T=-10 - 20°C;
参考文献
Schelper, Michael; De Meijere, Armin
European Journal of Organic Chemistry, 2005 , # 3 p. 582 - 592
反应条件
lithium diisopropyl amide 2.) Et2O, 0-20 deg C;
参考文献
Orsini, F.; Pelizzoni, F.
Synthetic Communications, 1984 , vol. 14, # 9 p. 805 - 816
反应条件
hydrogenchloride; n-butyllithium; chloro-trimethyl-silane; lithium bromide; diisopropylamine in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; acetone
参考文献
The University of South Carolina
Patent: US5059695 A1, 1991 ;
反应条件
in tetrachloromethane dropwise addn. of a soln. of Br2 to a soln. of Ge-compound cooled to -60°C; distn.;
参考文献
Bogoradovskii, E. T.; Zavgorodnii, V. S.; Liepin'sh, E. E.; Birgele, I. S.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1991 , vol. 61, p. 1295 - 1306
Zhurnal Obshchei Khimii, 1991 , vol. 61, p. 1418 - 1429
反应条件
1: BuLi 2: PPh3; Br2 View Scheme
参考文献
Wright, Justin M.; Jones, Graham B.
Tetrahedron Letters, 1999 , vol. 40, # 43 p. 7605 - 7609
反应条件
n-butyllithium; bromine; triphenylphosphine Multistep reaction;
参考文献
Josien, Hubert; David, Bom; Curran, Dennis P.; Zheng, Yu-Huang; Chou, Ting-Chao
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 24 p. 3189 - 3194
参考文献
Eiter,K. et al.
Justus Liebigs Annalen der Chemie, 1978 , p. 658 - 674
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Bogoradovskii, E. T.; Zavgorodnii, V. S.; Liepin'sh, E. E.; Birgele, I. S.; Petrov, A. A.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 6.2 p. 1418 - 1429,1295 - 1306
反应条件
Yield given. Multistep reaction;
参考文献
Wu, Ruilian; Schumm, Jeffry S.; Pearson, Darren L.; Tour, James M.
Journal of Organic Chemistry, 1996 , vol. 61, # 20 p. 6906 - 6921
