1,1,1-三甲基-N-苯基哌啶合成路线 （共 76 条）
反应条件
triethylamine in benzene T=50 - 60°C; 5 h;
参考文献
Mizhiritskii, M. D.; Reikhsfel'd, V. O.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 7 p. 1547 - 1558,1373 - 1382
反应条件
1: aniline With n-butyllithium in diethyl ether
T=20°C; Inert atmosphere;
2: chloro-trimethyl-silane in diethyl ether
T=-60 - 20°C; 2 h; Inert atmosphere;
参考文献
Schulz, Axel; Villinger, Alexander; Westenkirchner, Andrea
Inorganic Chemistry, 2013 , vol. 52, # 19 p. 11457 - 11468
参考文献
Anderson, H. H.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5802 - 5803
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Gmelin Handbook: Si: MVol.C, 111, page 310 - 313
反应条件
ammonium chloride
10 h; Reflux;
参考文献
Novikov, Mikhail S.; Babkov, Denis A.; Paramonova, Maria P.; Chizhov, Alexander O.; Khandazhinskaya, Anastasia L.; Seley-Radtke, Katherine L.
Tetrahedron Letters, 2013 , vol. 54, # 6 p. 576 - 578
参考文献
Anderson, H. H.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5802 - 5803
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Sauer, R. O.; Hasek, R. H.
Journal of the American Chemical Society, 1946 , vol. 68, p. 241 - 244
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Gmelin Handbook: Si: MVol.C, 111, page 310 - 313
反应条件
in tetrahydrofuran
T=-50°C;
参考文献
Casarini, Antonella; Dembech, Pasquale; Lazzari, Dario; Marini, Elisabetta; Reginato, Gianna; et al.
Journal of Organic Chemistry, 1993 , vol. 58, # 21 p. 5620 - 5623
反应条件
in chloroform
T=60 - 75°C; 5 h;
参考文献
Kozyukov, V. P.; Mironova, N. V.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 9 p. 2022 - 2027,1633 - 1637
反应条件
in diethyl ether
T=100°C; 10 h;
参考文献
Wiberg, N.; Preiner, G.; Wagner, G.; Koepf, H.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 9 p. 1062 - 1074
参考文献
Mjoerne, O.
Svensk Kemisk Tidskrift, 1950 , vol. 62, p. 120 - 122
C. A., 1950 , p. 9342
反应条件
Cu(NO3)2*3H2O
T=20°C; 0.3 h; Neat (no solvent); chemoselective reaction;
参考文献
Shirini; Mashhadi-Nejad
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 3 p. 376 - 381
