in neat (no solvent)
heating P3N5 at 710 °C on passing in gaseous CF3SF5; flushing with N2 before and after react.; cooling the receivers with dry ice-actone;; fractional vac. distn.;;
in neat (no solvent)
heating P3N5 at 710 °C on passing in gaseous CF3SF5; flushing with N2 before and after react.; cooling the receivers with dry ice-actone;; fractional vac. distn.;;