双(三甲基硅基)亚磷酸盐合成路线 (共 20 条)
反应条件
triethylamine in benzene Substitution; 2 h;
参考文献
Saakyan
Russian Journal of General Chemistry, 1999 , vol. 69, # 11 p. 1712 - 1716
反应条件
sodium T=140 - 150°C; 20 h;
参考文献
Journal of Organic Chemistry, , vol. 46, # 10 p. 2097 - 2107
参考文献
Journal of Organic Chemistry, , vol. 46, # 10 p. 2097 - 2107
反应条件
orthophosphorus acid; triethylamine in tetrahydrofuran; diethyl ether
T=20°C; 2 h;
参考文献
Mahmoudkhani, Amir H.; Langer, Vratislav; Lindqvist, Oliver
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 10 p. 2159 - 2168
反应条件
in formamide
1 h; Inert atmosphereSchlenk technique;
参考文献
Wessjohann, Ludger A.; Dessoy, Marco A.
Polyhedron, 2014 , vol. 70, p. 133 - 137
反应条件
orthophosphorus acid; triethylamine in tetrahydrofuran; diethyl ether
6 h; Heating;
参考文献
Sekine, Mitsuo; Okimoto, Kiyomi; Yamada, Khoji; Hata, Tsujiaki
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2097 - 2107
反应条件
Zinc chloride in benzene
参考文献
Bridgestone Corporation
Patent: US6433237 B1, 2002 ;
反应条件
tris(pentafluorophenyl)-borane in toluene
T=20°C;
参考文献
Denis, Jean-Marc; Forintos, Henrietta; Szelke, Helga; Keglevich, Gyoergy
Tetrahedron Letters, 2002 , vol. 43, # 32 p. 5569 - 5571
反应条件
phosphonic acid diethyl ester in dichloromethane
T=20°C; 1 h;
参考文献
Lewkowski, Jaroslaw; Dziegielewski, Marek
Heteroatom Chemistry, 2009 , vol. 20, # 7 p. 431 - 435
参考文献
Issleib, Kurt; Balszuweit, Arno; Richter, Hans-Juergen; Tonk, Walter
Zeitschrift fuer Chemie (Stuttgart, Germany), 1983 , vol. 23, # 12 p. 434 - 436