1: phosphonic acid dimethyl ester With triethylamine in dichloromethane T=0°C; Inert atmosphere; 2: chloro-trimethyl-silane in dichloromethane T=0°C; 0.5 h; Inert atmosphere;
参考文献
De Blieck, Ann; Masschelein, Kurt G. R.; Dhaene, Frederic; Rozycka-Sokolowska, Ewa; Marciniak, Bernard; Drabowicz, Jozef; Stevens, Christian V.
Chemical Communications, 2010 , vol. 46, # 2 p. 258 - 260