4-碘-2,6-二硝基甲苯合成路线 （共 12 条）
反应条件
sulfuric acid; nitric acid T=0 - 90°C;
参考文献
Array Biopharma, Inc.
Patent: US2010/63066 A1, 2010 ;
Location in patent: Page/Page column 36 ;
反应条件
trichloroisocyanuric acid; sulfuric acid T=130°C; 2 h;
参考文献
Mendona, Gabriela Fonseca; Senra, Monica Rufino; Esteves, Pierre M.; De Mattos, Marcio C.S.
Applied Catalysis A: General, 2011 , vol. 401, # 1-2 p. 176 - 181
反应条件
sulfuric acid; chlorine; silver sulphate T=80 - 90°C; 192 h;
参考文献
Segura, Pascual; Bunnett, Joseph F.; Villanova, Laura
Journal of Organic Chemistry, 1985 , vol. 50, # 7 p. 1041 - 1045
参考文献
F. HOFFMANN-LA ROCHE AG
Patent: EP887346 A2, 1998 ;
EP 0887346 A2
反应条件
nitric acid T=10 - 15°C;
参考文献
Ruggli; Zaeslin
Helvetica Chimica Acta, 1936 , vol. 19, p. 434,437
参考文献
Goldschmidt; Hoenig
Chemische Berichte, 1886 , vol. 19, p. 2443
Chemische Berichte, 1887 , vol. 20, p. 199
反应条件
1: alcohol; H2S; ammonia View Scheme
参考文献
Parkes; Farthing
Journal of the Chemical Society, 1948 , p. 1275,1277
反应条件
Diazotization.Behandlung der Diazoniumsalz-Loesung mit CuCl in konz. wss. HCl;
参考文献
Cohen; Mc Candlish
Journal of the Chemical Society, 1905 , vol. 87, p. 1265
参考文献
Ruggli; Zaeslin
Helvetica Chimica Acta, 1936 , vol. 19, p. 434,437
反应条件
(NH4)2S in ethanol; water T=50°C; 2 h;
参考文献
Array Biopharma, Inc.
Patent: US2010/63066 A1, 2010 ;
Location in patent: Page/Page column 36 ;
